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ASTM D 4373 : 2014

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

View Superseded by
superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Standard Test Method for Rapid Determination of Carbonate Content of Soils

Available format(s)

Hardcopy , PDF

Superseded date

02-07-2021

Language(s)

English

Published date

24-06-2014

This test method covers the determination of carbonate content of soils and soft rock which can be readily broken down by mechanical effort. It is a gasometric method that uses a simple portable apparatus.

1.1This test method covers the determination of carbonate content of soils and soft rock which can be readily broken down by mechanical effort. It is a gasometric method that uses a simple portable apparatus. Results should be clearly stated as the calcite equivalent in percent because different carbonate species cover a wide range of percent calcite equivalent as shown below for a number of carbonates:

Species

Cation

Calcite
Equivalent, %

Magnesite

Mg

117.0

Dolomite

Ca, Mg

108.6

Calcite

Ca

100.0

Aragonite

Ca

100.0

Rhodocrosite

Mn

87.1

Siderite

Fe

86.4

Smithsonite

Zn

79.8

Witherite

Ba

50.7

Cerrusite

Pb

37.5


For example, a 100 % dolomite would be expected to yield 108.6 % calcite equivalent while 100 % siderite would yield only 86.4 % calcite equivalent. Calcite and aragonite reactions will typically complete within about 10 minutes. This method does not distinguish between the carbonate species and such determination must be made using quantitative chemical analysis methods such as atomic absorption.

1.2Units—The values stated in SI units are to be regarded as the standard.

1.3All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.

1.3.1The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user's objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precaution statements, see Section 8.

Committee
D 18
DocumentType
Test Method
Pages
5
PublisherName
American Society for Testing and Materials
Status
Superseded
SupersededBy
Supersedes

ASTM D 4753 : 2002 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 653 : 2007 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 4753 : 2015 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 3740 : 2012 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2019 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2004 : REV A : EDT 1 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2008 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 6026 : 2013 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 6026 : 2006 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 1999 : REV C Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3042 : 2003 Standard Test Method for Insoluble Residue in Carbonate Aggregates
ASTM D 4753 : 1995 Standard Specification for Evaluating, Selecting, and Specifying Balances and Scales for Use in Soil, Rock, and Construction Materials Testing
ASTM D 3042 : 2009 : R2015 Standard Test Method for Insoluble Residue in Carbonate Aggregates
ASTM D 653 : 2020 : EDT 1 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 3042 : 2017 Standard Test Method for Insoluble Residue in Carbonate Aggregates
ASTM D 6026 : 1999 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2011 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 6026 : 2001 : EDT 1 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2010 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 6026 : 1996 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3740 : 2004 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 4753 : 2007 Standard Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction Materials Testing
ASTM D 3740 : 2001 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 653 : 2021 Standard Terminology Relating to Soil, Rock, and Contained Fluids
ASTM D 3740 : 2012 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3740 : 2003 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
ASTM D 3042 : 1997 Standard Test Method for Insoluble Residue in Carbonate Aggregates
ASTM D 6026 : 2001 Standard Practice for Using Significant Digits in Geotechnical Data
ASTM D 3042 : 2009 Standard Test Method for Insoluble Residue in Carbonate Aggregates
ASTM D 3740 : 2004 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction

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