Standard Test Methods of Chemical Analysis of Sulfonated and Sulfated Oils

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

25-07-2023

Publisher

American Society for Testing and Materials

1.1These test methods cover the chemical analysis of sulfonated and sulfated oils. The analytical procedures appear in the following order:

	Section

Moisture:
Test Method A. Water by Distillation with Volatile Solvent	4 – 9
Test Method B. Moisture and Volatile Matter by Hot-Plate Method	10 – 14
Organically Combined Sulfuric Anhydride:
Test Method A. Titration Test	15 – 19
Test Method B. Extraction-Titration Test	20 – 24
Test Method C. Ash-Gravimetric Test (in the Presence of True Sulfonates)	25 – 28
Total Desulfated Fatty Matter	29 – 32
Total Active Ingredients	33 – 36
Unsaponifiable Nonvolatile Matter	37 – 41
Inorganic Salts	42 – 46
Total Alkalinity	47 – 49
Total Ammonia	50 – 52
Acidity as Free Fatty Acids or Acid Number:
Test Method A. In the Absence of Ammonium or Triethanolamine Soaps	53 – 56
Test Method B. In the Presence of Dark Colored Oils but in the Absence of Ammonium or Triethanolamine Soaps (Brine Test)	57 – 60
Test Method C. In the Presence of Ammonium or Triethanolamine Soaps	61 – 63
Water-Immiscible Organic Solvents Volatile with Steam	64 – 70

1.2The values stated in inch-pound units are to be regarded as the standard. The metric equivalents of inch-pound units may be approximate.

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage.

1.4This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee	D 12
DocumentType	Test Method
Pages	12
PublisherName	American Society for Testing and Materials
Status	Current
Supersedes	ASTM D 500 : 1995 : R2016

ASTM D 5352 : 1995 : R2019	Standard Test Method for Determination of Organically Combined Sulfuric Anhydride Ash-Gravimetric, Test Method C
ASTM D 5349 : 2019	Standard Test Method for Determination of the Moisture and Volatile Content of Sulfonated, Sulfated Oils and Fatliquors by Oven Method
ASTM D 5354 : 1995 : R2020	Standard Test Method for Determination of Total Active Ingredients in Sulfonated and Sulfated Oils
ASTM D 5351 : 1993 : R2021	Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Extraction Titration, Test Method B
ASTM D 5353 : 1995 : R2019	Standard Test Method for Determination of Total Desulfated Fatty Matter
ASTM D 5350 : 1995 : R2019	Standard Test Method for Determination of Organically Combined Sulfuric Anhydride by Titration, Test Method A
ASTM D 5348 : 1995 : R2019	Standard Test Method for Determination of the Moisture Content of Sulfonated and Sulfated Oils by Distillation with Xylene