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EN 16857:2017

Current

Current

The latest, up-to-date edition.

Foodstuffs - Determination of benzene in soft drinks, other beverages and vegetable-based infant foods by headspace gas chromatography mass spectrometry (HS-GC-MS)

Published date

03-05-2017

European foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus
6 Procedure
7 HS-GC-MS analysis
8 Calculation
9 Precision data
10 Test report
Annex A (informative) - Typical chromatograms
Annex B (informative) - Precision data
Bibliography

This European Standard specifies a method for the determination of benzene in soft drinks, other beverages and vegetable-based infant foods, by headspace gas chromatography mass spectrometry (HS-GC-MS). The method has been validated in an interlaboratory study via the analysis of spiked samples of carbonated soft drink, still fruit-based drink, carbonated fruit-based drink, vegetable and fruit juice containing carrot, infant food vegetable based and infant food containing meat, ranging from 1,9 µg/kg to 18,6 µg/kg. However, linearity of the instrument response was proven for the concentration range from 0,5 µg/kg to 20 µg/kg. The limit of quantification (LOQ) depends on the instrument but can generally be expected to be in the range from 0,5 µg/kg to 1,0 µg/kg.

Committee
CEN/TC 275
DevelopmentNote
Supersedes PREN 16857. (05/2017)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
NS EN 16857 : 2017 Identical
NEN EN 16857 : 2017 Identical
PN EN 16857 : 2017 Identical
UNE-EN 16857:2018 Identical
DIN EN 16857:2015-05 (Draft) Identical
NF EN 16857 : 2017 Identical
DIN EN 16857:2017-07 Identical
UNI EN 16857 : 2017 Identical
BS EN 16857:2017 Identical
I.S. EN 16857:2017 Identical
DIN EN 16857 E : 2017 Identical
SN EN 16857 : 2017 Identical

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
EN ISO 1042 : 1999 LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)

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