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I.S. EN 16277:2012

Current

Current

The latest, up-to-date edition.

ANIMAL FEEDING STUFFS - DETERMINATION OF MERCURY BY COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CVAAS) AFTER MICROWAVE PRESSURE DIGESTION (EXTRACTION WITH 65% NITRIC ACID AND 30% HYDROGEN PEROXIDE)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2012

Preview

For Harmonized Standards, check the EU site to confirm that the Standard is cited in the Official Journal.

Only cited Standards give presumption of conformance to New Approach Directives/Regulations.

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents
5 Apparatus and equipment
6 Procedure
7 Calculation
8 Precision
9 Test report
Annex A (informative) - Results of the interlaboratory tests
Annex B (informative) - Flowchart - Determination of mercury
        by CVAAS after microwave digestion
Annex C (informative) - Alternative digestion procedure with
        the same extraction efficiency: Acid digestion with a
        mixture of 65% nitric acid and 70% perchloric acid
        (7:3 v/v) at atmospheric pressure
Annex D (informative) - Alternative digestion procedure with
        the same extraction efficiency: Acid digestion with a
        mixture of 65% nitric acid, 37% hydrochloric acid
        and 30% hydrogen peroxide under reflux
Bibliography

Provides a method for the determination of mercury in animal feeding stuffs by Cold-Vapour Atomic Absorption Spectrometry (CVAAS) after microwave pressure digestion.

DocumentType
Standard
Pages
20
PublisherName
National Standards Authority of Ireland
Status
Current

Standards Relationship
EN 16277 : 2012 Identical

EN 1483:2007 Water quality - Determination of mercury - Method using atomic absorption spectrometry
ISO 6497:2002 Animal feeding stuffs Sampling
EN 15550:2017 Animal feeding stuffs: Methods of sampling and analysis - Determination of cadmium and lead by graphite furnace atomic absorption spectrometry (GF-AAS) after pressure digestion
EN ISO 6498:2012 Animal feeding stuffs - Guidelines for sample preparation (ISO 6498:2012)
EN 13806:2002 Foodstuffs - Determination of trace elements - Determination of mercury by cold-vapour atomic absorption spectrometry (CVAAS) after pressure digestion
EN 13804:2013 Foodstuffs - Determination of elements and their chemical species - General considerations and specific requirements
EN 13805:2014 Foodstuffs - Determination of trace elements - Pressure digestion
EN ISO 6497 : 2005 ANIMAL FEEDING STUFFS - SAMPLING
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15621:2017 Animal feeding stuffs: Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, sulphur, iron, zinc, copper, manganese and cobalt after pressure digestion by ICP-AES

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