WATER QUALITY - PROTOCOL FOR THE INITIAL METHOD PERFORMANCE ASSESSMENT IN A LABORATORY

Published date

12-01-2013

Publisher

Avant-propos
1 Domaine d'application
2 Références normatives
3 Termes, définitions et symboles
  3.1 Vocabulaire général
  3.2 Vocabulaire propre au présent document
4 Principe
  4.1 Portée de l'évaluation intralaboratoire
  4.2 Organisation des protocoles de mesure
5 Évaluation des performances d'une méthode dans le
  laboratoire
  5.1 Étude de la fonction d'étalonnage: plan d'expériences
      de type A
  5.2 Étude d'une limite de quantification présupposée de
      la méthode: plan B
  5.3 Étude des rendements: plan d'expériences de type C
  5.4 Étude des interférences
  5.5 Étude de l'exactitude: plan d'expériences de type D
6 Résumé de l'évaluation initiale
Annexe A (normative) Calcul des paramètres d'exactitude
Annexe B (informative) Fractile de la loi de Fisher
Annexe C (informative) Calcul de la puissance du test et
         du risque bêta pour l'étude de l'exactitude
Annexe D (informative) Exemple
Annexe E (informative) Conduite des calculs avec un logiciel
Bibliographie

Ce document a pour objet de définir un protocole d'évaluation initiale d'une méthode quantitative, employée dans un laboratoire, dans le domaine de l'analyse physico-chimique de l'eau. Le présent document fournit en particulier des outils statistiques pour évaluer les différents critères choisis pour mener l'évaluation initiale d'une méthode développée ou adaptée par un laboratoire ou d'une méthode normalisée. Le responsable de l'évaluation pourra ultérieurement utiliser tout moyen d'ordre technique ou statistique sur l'évaluation des différents critères.

DevelopmentNote	Indice de classement: T90-210PR. XP NFT 90 210 December 1999. PR NFT 90 210 September 2008. (09/2008) PR NFT 90 210 June 2017. (06/2017)
DocumentType	Standard
PublisherName	Association Francaise de Normalisation
Status	Current

DIN EN 45545-2:2016-02	RAILWAY APPLICATIONS - FIRE PROTECTION ON RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAVIOUR OF MATERIALS AND COMPONENTS
BS EN 45545-2 : 2013	RAILWAY APPLICATIONS - FIRE PROTECTION ON RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAVIOUR OF MATERIALS AND COMPONENTS
S.R. CEN/TS 16800:2015	GUIDELINE FOR THE VALIDATION OF PHYSICO-CHEMICAL ANALYTICAL METHODS
CEN/TS 16800:2015	GUIDELINE FOR THE VALIDATION OF PHYSICO-CHEMICAL ANALYTICAL METHODS
FD T90 187-1 : 2010 FD	WATER QUALITY - DETERMINATION OF GLYPHOSATE AND AMINOMETHYLPHOSPHONIC ACID (AMPA) - PART 1: ANALYSIS METHOD BY LIQUID CHROMATOGRAPHY WITH FLUORIMETRIC DETECTION USING POST-COLUMN DERIVATION
XP T90 220 : 2003 XP	WATER QUALITY - PROTOCOL FOR THE ESTIMATION OF UNCERTAINTY ASSOCIATED TO AN ANALYSIS RESULT FOR PHYSICO-CHEMICAL ANALYSIS METHOD
FD X07 022 : 2004 FD	METROLOGY AND STATISTICAL APPLICATIONS - USE OF UNCERTAINTIES OF MEASUREMENTS: PRESENTATION OF SOME CASES AND COMMON PRACTICES
S.R. CEN/TS 45545-2:2009	RAILWAY APPLICATIONS - FIRE PROTECTION ON RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAVIOUR OF MATERIALS AND COMPONENTS
DIN EN 14902 E : 2005	AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF PB, CD, AS AND NI IN THE PM10 FRACTION OF SUSPENDED PARTICULATE MATTER
EN 45545-2:2013+A1:2015	Railway applications - Fire protection on railway vehicles - Part 2: Requirements for fire behaviour of materials and components
UNI CEI EN 45545-2 : 2013	RAILWAY APPLICATIONS - FIRE PROTECTION ON RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAUVIOR OF MATERIALS AND COMPONENTS
10/30216687 DC : 0	BS EN 45545-2 - RAILWAY APPLICATIONS - FIRE PROTECTION ON RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAVIOUR OF MATERIALS AND COMPONENTS
FD T90 230 : 2015 FD	WATER QUALITY - CHARACTERIZATION OF ANALYTICAL METHODS - GUIDE FOR SELECTION OF A MATRIX REPRESENTATIVE OF A SCOPE OF APPLICATION
PD CEN/TS 16800:2015	Guideline for the validation of physico-chemical analytical methods
NFX 70 100-1 : 2006	FIRE TESTS - ANALYSIS OF GASEOUS EFFLUENTS - PART 1: METHODS FOR ANALYSING GASES STEMMING FROM THERMAL DEGRADATION
BS EN 14902:2005	Ambient air quality. Standard method for the measurement of Pb, Cd, AS, and Ni in the PM 10 fraction of suspended particulate matter
NFM 60 335 : 2011	GUIDELINE STANDARD FOR THE ANALYSIS OF 15 ITEMS OF INTEREST FOR THE CHEMICAL CHARACTERISATION OF RADIOACTIVE WASTE
UNI CEI CEN/TS 45545-2 : 2009	RAILWAY APPLICATIONS - FIRE PROTECTION OF RAILWAY VEHICLES - PART 2: REQUIREMENTS FOR FIRE BEHAVIOUR OF MATERIALS AND COMPONENTS
NFT 90 554 : 2007	WATER QUALITY - ON-LINE SENSORS/ANALYSING EQUIPMENT FOR LOW TURBIDITY MEASUREMENT - SPECIFICATIONS AND PERFORMANCE TESTS
DD CEN/TS 45545-2:2009	Railway applications. Fire protection on railway vehicles Requirements for fire behaviour of materials and components
DIN EN 14902:2005-10	AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF PB, CD, AS AND NI IN THE PM10 FRACTION OF SUSPENDED PARTICULATE MATTER
EN 14902:2005/AC:2006	AMBIENT AIR QUALITY - STANDARD METHOD FOR THE MEASUREMENT OF PB, CD, AS AND NI IN THE PM10 FRACTION OF SUSPENDED PARTICULATE MATTER
NFX 43 303 : 2011	STATIONARY SOURCE EMISSIONS - DETERMINATION OF AMMONIA (NH3)
FD X07 008 : 2008 FD	METROLOGY - ARBORESCENCE OF STANDARDS AND WORK ON METROLOGY ('ROAD MAP' OF STANDARDS)
NFX 07 008 : 2008 FD	METROLOGY - ARBORESCENCE OF STANDARDS AND WORK ON METROLOGY ("ROAD MAP" OF STANDARDS)
CEN/TS 45545-2:2009	Railway applications - Fire protection on railway vehicles - Part 2: Requirements for fire behaviour of materials and components

NF ISO 5725-2 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 2: BASIC METHOD FOR THE DETERMINATION OF REPEATABILITY AND REPRODUCIBILITY OF A STANDARD MEASUREMENT METHOD
NF ISO 5725-1 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 1: GENERAL PRINCIPLES AND DEFINITIONS
ISO/TR 13530:1997	Water quality Guide to analytical quality control for water analysis
NF ISO 5725-3 : 1994	APPLICATION OF STATISTICS - ACCURACY (TRUENESS AND PRECISION) OF MEASUREMENT METHODS AND RESULTS - PART 3: INTERMEDIATE MEASURES OF THE PRECISION OF A STANDARD MEASUREMENT METHOD