Fat and oil derivatives. Fatty acid methyl ester (FAME). Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-31-2007

Publisher

British Standards Institution

Foreword
1 Scope
2 Normative references
3 Principle
4 Chemicals
5 Apparatus
6 Sampling
7 Preparation of the calibration solutions and the
   blank solution
   7.1 General
   7.2 Blank solution
   7.3 Calibration solution with a nominal element
       content of 0,5 mg/kg
   7.4 Calibration solution with a nominal element
       content of 1 mg/kg
   7.5 Calibration solution with a nominal element
       content of 5 mg/kg
   7.6 Calibration solution with a nominal element
       content of 10 mg/kg
8 Calibration
   8.1 General
   8.2 Calibration
   8.3 Check of calibration
9 Sample analysis
   9.1 Sample preparation
   9.2 Measurement
10 Calculation
11 Results
12 Precision
   12.1 Repeatability
   12.2 Reproducibility
13 Test report

Defines a procedure for the direct determination of the soap building elements Calcium (Ca), Magnesium (Mg), Sodium (Na) and Potassium (K) in fatty acid methyl esters (FAME) by ICP OES at levels of about 1 mg/kg to 10 mg/kg.

Committee	PTI/13
DevelopmentNote	Also numbered as BS 2000-547(2006). Supersedes 02/123664 DC (02/2007)
DocumentType	Standard
Pages	12
PublisherName	British Standards Institution
Status	Current
Supersedes	02/123664 DC : DRAFT SEP 2002

Standards	Relationship
NS EN 14538 : 1ED 2006	Identical
NF EN 14538 : 2007	Identical
SN EN 14538 : 2006	Identical
NBN EN 14538 : 2006	Identical
EN 14538:2006	Identical
UNI EN 14538 : 2006	Identical
UNE-EN 14538:2006	Identical
NEN EN 14538 : 2006	Identical
I.S. EN 14538:2006	Identical
DIN EN 14538:2006-09	Identical
DIN EN 14538 E : 2006	Identical

ISO 3171:1988	Petroleum liquids — Automatic pipeline sampling
ISO 3170:2004	Petroleum liquids — Manual sampling
EN ISO 3170:2004	Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 3171:1999	Petroleum liquids - Automatic pipeline sampling (ISO 3171:1988)

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BS EN 14538:2006

Fat and oil derivatives. Fatty acid methyl ester (FAME). Determination of Ca, K, Mg and Na content by optical emission spectral analysis with inductively coupled plasma (ICP OES)

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Abstract

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