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ASTM D 6800 : 2018

Current

Current

The latest, up-to-date edition.

Standard Practice for Preparation of Water Samples Using Reductive Precipitation Preconcentration Technique for ICP-MS Analysis of Trace Metals

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

07-01-2018

1.1Toxic elements may be present in ambient waters and may enter the food chain via uptake by plants and animals; the actual concentrations of toxic metals are usually sub-ng/mL. The U.S. EPA has published its Water Quality Standards in the U.S. Federal Register 40 CFR 131.36, Minimum requirements for water quality standards submission, Ch. I (7-1-00 Edition), see Annex, Table A1.1. The U.S. EPA has also developed Method 1640 to meet these requirements, see Annex, Table A1.2.

1.2Inductively Coupled Plasma Mass Spectroscopy (ICP-MS) is a technique with sufficient sensitivity to routinely measure toxic elements in ambient waters, both fresh and saline (Test Method D5673). However saline and hard water matrices pose analytical challenges for direct multielement analysis by ICP-MS at the required sub-ng/mL levels.

1.3This practice describes a method used to prepare water samples for subsequent multielement analysis using ICP-MS. The practice is applicable to seawater and fresh water matrices, which may be filtered or digested. Samples prepared by this method have been analyzed by ICP-MS for the elements listed in Annex, Table A1.3).

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 19
DocumentType
Standard Practice
Pages
9
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 5810 : 1996 : R2021 Standard Guide for Spiking into Aqueous Samples
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 5673 : 2015 Standard Test Method for Elements in Water by Inductively Coupled Plasma—Mass Spectrometry
ASTM D 5673 : 1996 Standard Test Method for Elements in Water by Inductively Coupled Plasma—Mass Spectrometry
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5847 : 2022 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 5810 : 1996 Standard Guide for Spiking into Aqueous Samples
ASTM D 5810 : 1996 : R2015 Standard Guide for Spiking into Aqueous Samples

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