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CEN
CEN/TR 16269:2011

CEN/TR 16269:2011

Current

Current

The latest, up-to-date edition.

Ambient air - Guide for the measurement of anions and cations in PM2,5

Published date

09-21-2011

Publisher

Comite Europeen de Normalisation

Foreword
Introduction
1 Scope
2 Terms and definitions
3 Symbols and abbreviations
4 Principle
5 Apparatus
6 Sampling, transport and storage
7 Analysis
8 Calculation of results
9 Quality control
10 Measurement uncertainty
11 Artefacts and interferences
12 Reporting of results
Annex A (informative) - Example of a closed vessel
        microwave digestion procedure to determine
        elements in the water-insoluble fraction
        of PM[2,5]
Annex B (informative) - Preparation of stock standard
        solution
Annex C (informative) - Uncertainty budget
Annex D (informative) - Data quality objectives
Annex E (informative) - Reagents
Bibliography

This CEN Technical Report specifies a method for the determination of the mass of water soluble NO3-, SO42-, Cl-, NH4+, Na+, K+, Mg2+, Ca2+ in PM2,5 samples which can be used to comply with Directive 2008/50/EC. This CEN Technical Report describes a measurement method which comprises sampling of anions and cations as part of the PM2,5 particulate phase, sample extraction and analysis of anions and cations by ion chromatography. Alternately, cations, excluding ammonium can be analysed by inductively coupled plasma optical emission spectrometry (ICP-OES).This CEN Technical Report may be used at rural background monitoring sites that are in accordance with the requirements of Directive 2008/50/EC. However, since this CEN Technical Report has not been validated in the field for these, or any other, monitoring site types, it may be considered equally applicable to all site types.NOTEThe detection limits described in this CEN technical report method will be limited by the noise level of the detector and the variability of the mass in laboratory blank filters rather than by the concentrations of anions and cations in ambient air.

Committee
CEN/TC 264
DocumentType
Technical Report
PublisherName
Comite Europeen de Normalisation
Status
Current

I.S. EN 16909:2017 AMBIENT AIR - MEASUREMENT OF ELEMENTAL CARBON (EC) AND ORGANIC CARBON (OC) COLLECTED ON FILTERS
BS EN 12341:2014 Ambient air. Standard gravimetric measurement method for the determination of the PM<sub>10</sub> or PM<sub>2</sub>$d,<sub>5</sub> mass concentration of suspended particulate matter
EN 12341:2014 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
BS EN 16909:2017 Ambient air. Measurement of elemental carbon (EC) and organic carbon (OC) collected on filters
UNE-EN 12341:2015 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter
DIN EN 12341:1999-03 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM[10] OR PM[2],[5] MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
I.S. EN 12341:2014 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM[10] OR PM[2,5] MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
DIN EN 16909:2017-06 AMBIENT AIR - MEASUREMENT OF ELEMENTAL CARBON (EC) AND ORGANIC CARBON (OC) COLLECTED ON FILTERS
DIN EN 16909 E : 2017 AMBIENT AIR - MEASUREMENT OF ELEMENTAL CARBON (EC) AND ORGANIC CARBON (OC) COLLECTED ON FILTERS
DIN EN 12341:2014-08 Ambient air - Standard gravimetric measurement method for the determination of the PM or PM mass concentration of suspended particulate matter
UNI EN 12341 : 2014 AMBIENT AIR - STANDARD GRAVIMETRIC MEASUREMENT METHOD FOR THE DETERMINATION OF THE PM10 OR PM2,5 MASS CONCENTRATION OF SUSPENDED PARTICULATE MATTER
15/30314076 DC : 0 BS EN 16909 - AMBIENT AIR - MEASUREMENT OF ELEMENTAL CARBON (EC) AND ORGANIC CARBON (OC) DEPOSITED ON FILTERS
EN 16909:2017 Ambient air - Measurement of elemental carbon (EC) and organic carbon (OC) collected on filters
DIN EN 16909:2015-10 (Draft) AMBIENT AIR - MEASUREMENT OF ELEMENTAL CARBON (EC) AND ORGANIC CARBON (OC) COLLECTED ON FILTERS

EN 13274-7:2008 Respiratory protective devices - Methods of test - Part 7: Determination of particle filter penetration
EN ISO 11885:2009 Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (ISO 11885:2007)
EN 14907:2005 Ambient air quality - Standard gravimetric measurement method for the determination of the PM2,5 mass fraction of suspended particulate matter
ISO/IEC Guide 99:2007 International vocabulary of metrology Basic and general concepts and associated terms (VIM)
EN 1822-1:2009 High efficiency air filters (EPA, HEPA and ULPA) - Part 1: Classification, performance testing, marking
EN ISO 10304-1:2009 Water quality - Determination of dissolved anions by liquid chromatography of ions - Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite, phosphate and sulfate (ISO 10304-1:2007)
EN ISO 14911 : 1999 WATER QUALITY - DETERMINATION OF DISSOLVED LI+, NA+, NH4+, K+, MN2+, CA2+, MG2+, SR2+ AND BA2+ USING ION CHROMATOGRAPHY - METHOD FOR WATER AND WASTE WATER
EN 12341:2014 Ambient air - Standard gravimetric measurement method for the determination of the PM10 or PM2,5 mass concentration of suspended particulate matter

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