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CEN
ENV 13800:2000

ENV 13800:2000

Withdrawn

Withdrawn

A Withdrawn Standard is one, which is removed from sale, and its unique number can no longer be used. The Standard can be withdrawn and not replaced, or it can be withdrawn and replaced by a Standard with a different number.

Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), without separation of the lead matrix

Withdrawn date

08-26-2022

Published date

07-19-2000

Publisher

Comite Europeen de Normalisation

Foreword
1 Scope
2 Normative references
3 Principle
      3.1 Dissolution
      3.2 Instrumental techniques
4 Apparatus
      4.1 General
      4.2 Volumetric glassware
      4.3 Plastic ware
      4.4 Instruments
5 Reagents
      5.1 General
      5.2 Nitric acid (HNO3)
      5.3 Tartaric acid solution (C4H6O6) 300 g/l
      5.4 Hydrochloric acid (HCI)
      5.5 Fluoboric acid (HBF4)
      5.6 Lead for matrix matching
      5.7 Standard solutions
6 Sampling and sample preparation
7 Procedure
      7.1 Preparation of the test solution
      7.2 Preparation of the blank test solution
      7.3 Dilution of the test solutions and of the blank
             test solution
8 Determination of elements by FAAS
      8.1 Preparation of calibration solutions
      8.2 Calibration, measurements and results
9 Determination of elements by ICP-ES
      9.1 Preparation of calibration solutions
      9.2 Calibration, measurements and results
10 Test report

This European Prestandard specifies methods of analysis using flame atomic absorption spectrometry (FAAS) and inductively coupled plasma emission spectrometry (ICP-ES) for the determination of element contents in lead and lead alloys for the ranges given in Table 1.These methods are intended as the definitive methods in case of dispute for the determination of elements at low content in lead. They are also recommended for the analysis of Certified Reference Materials (CRM) and Reference Materials (RM) which are used in analysis according to ENV 12908.

Committee
CEN/TC 306
DocumentType
Standard Recommendation
PublisherName
Comite Europeen de Normalisation
Status
Withdrawn

Standards Relationship
NBN ENV 13800 : 2000 Identical
UNI ENV 13800 : 2002 Identical
NEN NVN ENV 13800 : 2000 Identical
I.S. ENV 13800:2000 Identical
DIN V ENV 13800:2000-11 Identical
DD ENV 13800:2000 Identical

DIN 17640-1:2004-02 Lead alloys for general purposes
ENV 14029:2001 Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix
ENV 14138:2001 Lead and lead alloys - Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation by co-precipitation
DD ENV 14138:2001 Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emissions spectrometry (ICP-ES), after separation by co-precipitation
DD ENV 14029:2001 Lead and lead alloys. Analysis by flame atomic absorption spectrometry (FAAS) or inductively coupled plasma emission spectrometry (ICP-ES), after separation of the lead matrix
I.S. ENV 14138:2002 LEAD AND LEAD ALLOYS - ANALYSIS BY FLAME ATOMIC ABSORPTION SPECTROMETRY (FAAS) OR INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY (ICP-ES), AFTER SEPARATION BY CO-PRECIPITATION

EN 12402 : 1999 LEAD AND LEAD ALLOYS - METHODS OF SAMPLING FOR ANALYSIS
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 648:2008 Laboratory glassware — Single-volume pipettes
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
ENV 12908:1997 Lead and lead alloys - Analysis by Optical Emission Spectrometry (OES) with spark excitation

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