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    AS 1038.6.3.3-1997

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    Coal and coke - Analysis and testing Higher rank coal - Ultimate analysis - Total sulfur - Infrared method (Reconfirmed 2013)

    Available format(s):  Hardcopy, PDF 1 User, PDF 3 Users, PDF 5 Users, PDF 9 Users

    Language(s):  English

    Published date:  05-12-1997

    Publisher:  Standards Australia

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    Description - (Show below) - (Hide below)

    This Standard has been reconfirmed. To view or download the Reconfirmation Notice please click here.

    Table of Contents - (Show below) - (Hide below)

    1 - AS 1038.6.3.3-1997 COAL AND COKE - ANALYSIS AND TESTING - HIGHER RANK COAL - ULTIMATE ANALYSIS - TOTAL SULFUR - INFRARED MET
    4 - PREFACE
    5 - CONTENTS
    6 - FOREWORD
    7 - 1 SCOPE
    7 - 2 REFERENCED DOCUMENTS
    7 - 3 DEFINITIONS
    7 - 3.1 Repeatability (r)
    7 - 4 PRINCIPLE
    8 - 5 SAFETY
    8 - 6 REAGENTS
    8 - 6.1 Magnesium perchlorate, anhydrous, granular
    8 - 6.2 Reference coal samples
    8 - 6.3 Glass wool
    8 - 6.4 Oxygen
    8 - 7 APPARATUS
    8 - 7.1 Resistance furnace
    8 - 7.2 Combustion tube
    8 - 7.3 Combustion boats
    8 - 7.4 Combustion gas purification train
    8 - 7.5 Infrared measurement system
    8 - 8 SAMPLE
    8 - 9 PROCEDURE
    8 - 9.1 Calibration
    8 - 9.2 Determination
    9 - 10 REPORTING OF RESULTS
    9 - 11 PRECISION
    9 - 12 TEST REPORT
    10 - APPENDIX A - STATISTICAL DATA FOR DETERMINATION OF THE TOTAL SULFUR CONTENT OF HIGHER RANK COALS

    Abstract - (Show below) - (Hide below)

    Sets out a method by heating in oxygen, converting to sulfur dioxide and measuring by infrared detection, for the determination of total sulfur in the analysis sample of higher rank coal and coke.

    Scope - (Show below) - (Hide below)

    This Standard sets out a method for the determination of total sulfur in the analysis sample of higher rank coal by the infrared method.This method has been shown to be applicable to samples having ash values less than 40% and sulfur levels up to 6%. Samples having ash levels greater than approximately 40% may give low results.

    General Product Information - (Show below) - (Hide below)

    Committee MN/1
    Document Type Standard
    Product Note Reconfirmed 06-08-2013
    Publisher Standards Australia
    Status Current
    Supersedes

    History - (Show below) - (Hide below)

    First published an AS 1038.6.3.3-1986.* Second edition 1997.Reconfirmed 2013. Originated as AS 1038.6.3.3-1986. Second edition 1997.

    Standards Referenced By This Book - (Show below) - (Hide below)

    AS 1038.4-2006 Coal and coke - Analysis and testing Coke - Proximate analysis
    AS 4264.2-1996 Coal and coke - Sampling Coke - Sampling procedures (Reconfirmed 2013)
    AS 2706-1984 Numerical values - Rounding and interpretation of limiting values
    AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013)
    AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
    AS 1038.3-2000 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
    AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
    AS 2706-2003 Numerical values - Rounding and interpretation of limiting values (Reconfirmed 2018)
    AS 1038.6.1-1997 Coal and coke - Analysis and testing Higher rank coal and coke - Ultimate analysis - Carbon and hydrogen (Reconfirmed 2013)
    AS 1038.3-1989 Coal and coke - Analysis and testing - Proximate analysis of higher rank coal
    AS 1038.4-1995 Coal and coke - Analysis and testing Coke - Proximate analysis
    AS 4264.1-1995 Coal and coke - Sampling Higher rank coal - Sampling procedures

    Standards Referencing This Book - (Show below) - (Hide below)

    TR 2.12A-2 Certified reference materials - Coal - Preparation and certification of ASCRM 012A-2
    AS 1038.11-2002 Coal and coke - Analysis and testing Coal - Forms of sulfur (Reconfirmed 2013)
    AS 2096-1987 Classification and coding systems for Australian coals (Reconfirmed 2013)
    AS 1038.16-2005 Coal and coke - Analysis and testing Assessment and reporting of results (Reconfirmed 2016)
    AS 2519-1993 Guide to the technical evaluation of higher rank coal deposits (Reconfirmed 2013)
    TR 2.12C-2 Certified reference materials - Coal - Preparation and certification of ASCRM 012C-2
    TR 2.12B-3 Reference Materials - Coal - Preparation of ASRM 012B-3
    AS 1038.16-1996 Coal and coke - Analysis and testing - Assessment and reporting of results
    TR 2.12B-2 Certified reference materials - Coal - Preparation and certification of ASCRM-012B-2
    TR 2.12B-4-2009 Coal - Preparation of ASCRM 012B-3
    TR 2.12C-3-2008 Certified reference materials Coal - Preparation and certification of ASCRM 012C-3
    AS 2418-1995 Coal and coke - Glossary of terms (Reconfirmed 2013)
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