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ASTM D 7065 : 2017

Current

Current

The latest, up-to-date edition.

Standard Test Method for Determination of Nonylphenol, Bisphenol A, p-tert-Octylphenol, Nonylphenol Monoethoxylate and Nonylphenol Diethoxylate in Environmental Waters by Gas Chromatography Mass Spectrometry

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

15-12-2017

1.1This test method covers determination of nonylphenol (NP), nonylphenol ethoxylate (NP1EO), nonylphenol diethoxylate (NP2EO), octylphenol (OP), and bisphenol A (BPA) that are partitioned into organic solvent, separated using gas chromatography and detected with mass selective detection. These compounds or isomer mixtures are qualitatively and quantitatively determined by this test method. This test method adheres to selected ion monitoring mass spectrometry but full scan mass spectrometry has also been shown to work well under these conditions. Either analysis may be used.

1.2The method detection limit (MDL) and reporting limit (RL) for NP, NP1EO, NP2EO, OP, and BPA are listed in Table 1.

(A)MDL determined following the Code of Federal Regulations, 40 CFR Part 136, Appendix B.
(B)Lowest point of the reporting range is calculated from the LV1 concentration calibration standard in Table 4.

1.3The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.5This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 19
DocumentType
Test Method
Pages
14
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM F 2931 : 2019 Standard Guide for Analytical Testing of Substances of Very High Concern in Materials and Products

ASTM D 3694 : 1996 : R2011 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 5905 : 1998 : R2013 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1129 : 2003 Standard Terminology Relating to Water
ASTM D 1129 : 2013 Standard Terminology Relating to Water
ASTM D 1129 : 2013 : R2020 Standard Terminology Relating to Water
ASTM D 5847 : 1999 : REV A : EDT 1 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3694 : 1996 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 5905 : 1998 : R2018 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1129 : 2013 : R2020 : EDT 2 Standard Terminology Relating to Water
ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2007 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2006 Standard Terminology Relating to Water
ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 5847 : 2002 : R2012 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5905 : 1998 : R2008 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 3694 : 1996 : R2017 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2013 : R2020 : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 1999 : REV A Standard Terminology Relating to Water
ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3856 : 2011 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water
ASTM D 1129 : 2006 : REV A Standard Terminology Relating to Water
ASTM E 691 : 2023 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
ASTM D 5847 : 2002 : R2020 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 1129 : 2003 : REV A Standard Terminology Relating to Water
ASTM D 3694 : 1996 : R2004 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1129 : 2002 Standard Terminology Relating to Water
ASTM E 691 : 2022 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 1193 : 1991 Standard Specification for Reagent Water
ASTM D 5905 : 1998 : EDT 1 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 3856 : 1995 : R2006 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2004 Standard Terminology Relating to Water
ASTM D 5847 : 2022 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 3856 : 2011 : R2015 Standard Guide for Management Systems in Laboratories Engaged in Analysis of Water (Withdrawn 2024)
ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
ASTM D 3856 : 1995 : R2000 Standard Guide for Good Laboratory Practices in Laboratories Engaged in Sampling and Analysis of Water
ASTM D 1129 : 2002 : REV A Standard Terminology Relating to Water
ASTM D 5847 : 2002 Standard Practice for Writing Quality Control Specifications for Standard Test Methods for Water Analysis
ASTM D 5905 : 1998 : R2003 Standard Practice for the Preparation of Substitute Wastewater
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 1193 : 2006 Standard Specification for Reagent Water
ASTM D 1193 : 1999 Standard Specification for Reagent Water
ASTM D 1129 : 2010 Standard Terminology Relating to Water
ASTM D 1129 : 2006 : REV A : EDT 1 Standard Terminology Relating to Water
ASTM D 1129 : 2001 Standard Terminology Relating to Water
ASTM D 1129 : 2004 : EDT 1 Standard Terminology Relating to Water
ASTM D 3694 : 1996 : R2024 Standard Practices for Preparation of Sample Containers and for Preservation of Organic Constituents
ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water

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