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EN ISO 5983-2:2009

Current

Current

The latest, up-to-date edition.

Animal feeding stuffs - Determination of nitrogen content and calculation of crude protein content - Part 2: Block digestion and steam distillation method (ISO 5983-2:2009)

Published date

01-06-2009

Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
5 Reagents
6 Apparatus
7 Sampling
8 Preparation of test sample
9 Procedure
   9.1 General
   9.2 Test portion
   9.3 Determination
   9.4 Blank test
   9.5 Recovery tests
10 Calculation and expression of results
   10.1 Calculation
   10.2 Calculation of crude protein content
   10.3 Expression of crude protein content results
11 Precision
   11.1 Interlaboratory tests
   11.2 Repeatability
   11.3 Reproducibility
12 Test report
Annex A (informative) - Results of interlaboratory tests
Annex B (informative) - Results of a proficiency test; comparison
        of the colorimetric and potentiometric endpoint
        determination of the titration
Bibliography

ISO 5983-2:2009 specifies a method for the determination of nitrogen content of animal feeding stuffs according to the Kjeldahl method, and a method for the calculation of the crude protein content.It is suitable for use as a semi-micro rapid routine method using block digestion, copper catalyst, and steam distillation into boric acid.The method is applicable to the determination of greater than 0,5 % mass fraction Kjeldahl nitrogen in animal feeding stuffs, pet foods, and their raw materials.The method does not measure oxidized forms of nitrogen nor heterocyclic nitrogen compounds.The method does not distinguish between protein nitrogen and non-protein nitrogen.

Committee
CEN/TC 327
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

14/30301619 DC : 0 BS EN 15948 - CEREALS - DETERMINATION OF MOISTURE AND PROTEIN - METHOD USING NEAR-INFRARED-SPECTROSCOPY IN WHOLE KERNELS
DIN EN 15948:2015-06 CEREALS - DETERMINATION OF MOISTURE AND PROTEIN - METHOD USING NEAR-INFRARED-SPECTROSCOPY IN WHOLE KERNELS
UNE-EN 15948:2015 Cereals - Determination of moisture and protein - Method using Near-Infrared-Spectroscopy in whole kernels
I.S. EN 15948:2015 CEREALS - DETERMINATION OF MOISTURE AND PROTEIN - METHOD USING NEAR-INFRARED-SPECTROSCOPY IN WHOLE KERNELS
EN 15948:2015 Cereals - Determination of moisture and protein - Method using Near-Infrared-Spectroscopy in whole kernels
09/30201998 DC : 0 BS EN 15948 - CEREALS - DETERMINATION OF MOISTURE AND PROTEIN - METHOD USING NEAR-INFRARED-TRANSMITTANCE IN COMBINATION WITH AN ARTIFICIAL NEURAL NETWORK (ANN) PREDICTION MODEL AND ASSOCIATED DATABASE
BS EN 15948:2015 Cereals. Determination of moisture and protein. Method using Near-Infrared-Spectroscopy in whole kernels
08/30189315 DC : DRAFT SEP 2008 BS EN ISO 12099 - ANIMAL FEEDSTUFFS, CEREALS AND MILLED CEREAL PRODUCTS - GUIDELINES FOR THE APPLICATION OF NEAR INFRARED SPECTROMETRY

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
ISO 8655-5:2002 Piston-operated volumetric apparatus Part 5: Dispensers
ISO 1871:2009 Food and feed products General guidelines for the determination of nitrogen by the Kjeldahl method
ISO 5983-1:2005 Animal feeding stuffs Determination of nitrogen content and calculation of crude protein content Part 1: Kjeldahl method
ISO 385:2005 Laboratory glassware Burettes
ISO 6497:2002 Animal feeding stuffs Sampling
ISO 8655-2:2002 Piston-operated volumetric apparatus Part 2: Piston pipettes
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 6498:2012 Animal feeding stuffs — Guidelines for sample preparation
ISO 8655-3:2002 Piston-operated volumetric apparatus Part 3: Piston burettes

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