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  • ASTM D 2593 : 1993 : R2014

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    Standard Test Method for Butadiene Purity and Hydrocarbon Impurities by Gas Chromatography

    Available format(s):  Hardcopy, PDF

    Superseded date:  09-06-2023

    Language(s):  English

    Published date:  24-07-2014

    Publisher:  American Society for Testing and Materials

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    Abstract - (Show below) - (Hide below)

    CONTAINED IN VOL. 05.01, 2015 Specifies the determination of butadiene-1,3 purity and impurities such as propane, propylene, isobutane, n-butane, butene-1, isobutylene, propadiene, trans-butene-2, cis-butene-2, butadiene-1,2, pentadiene-1,4, and, methyl, dimethyl, ethyl, and vinyl acetylene in polymerization grade butadiene by gas chromatography.

    Scope - (Show below) - (Hide below)

    1.1This test method covers the determination of butadiene-1,3 purity and impurities such as propane, propylene, isobutane, n-butane, butene-1, isobutylene, propadiene, trans-butene-2, cis -butene-2, butadiene-1,2, pentadiene-1,4, and, methyl, dimethyl, ethyl, and vinyl acetylene in polymerization grade butadiene by gas chromatography. Impurities including butadiene dimer, carbonyls, inhibitor, and residue are measured by appropriate ASTM procedures and the results used to normalize the component distribution obtained by chromatography.

    Note 1:Other impurities present in commercial butadiene must be calibrated and analyzed. Other impurities were not tested in the cooperative work on this test method.

    Note 2:This test method can be used to check for pentadiene-1,4 and other C5s instead of Test Method D1088.

    1.2The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific warning statements, see 6.1 and 9.3.

    General Product Information - (Show below) - (Hide below)

    Committee D 02
    Development Note Also numbered as IP 194. (11/2004)
    Document Type Test Method
    Product Note Reconfirmed 2014
    Publisher American Society for Testing and Materials
    Status Superseded
    Superseded By
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 6691 : 2017 Standard Test Method for Determining Aerobic Biodegradation of Plastic Materials in the Marine Environment by a Defined Microbial Consortium or Natural Sea Water Inoculum
    ASTM D 2804 : 2002 : R2012 Standard Test Method for Purity of Methyl Ethyl Ketone By Gas Chromatography (Withdrawn 2021)
    ASTM D 3545 : 2006 : R2012 Standard Test Method for Alcohol Content and Purity of Acetate Esters by Gas Chromatography (Withdrawn 2021)
    ASTM D 2426 : 1993 : R2014 Standard Test Method for Butadiene Dimer and Styrene in Butadiene Concentrates by Gas Chromatography
    ASTM D 5274 : 2000 : R2014 Standard Guide for Analysis of 1,3–Butadiene Product
    ASTM D 3329 : 2003 : R2017 Standard Test Method for Purity of Methyl Isobutyl Ketone by Gas Chromatography

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 1088 : 1953 : R1978 Method of Test for Boiling Point Range of Polymerization-Grade Butadiene (Withdrawn 1983)
    IP 194 : 74(R1981) DETERMINATION OF BUTADIENE PURITY - GAS CHROMATOGRAPHY METHOD
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