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BS 5984:1980

Superseded

Superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

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superseded

A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.

Method for detection and determination of specified anti-oxidant additives in insulating oils

Available format(s)

Hardcopy , PDF

Superseded date

31-08-2010

Language(s)

English

Published date

29-08-1980

National foreword
Cooperating organizations
1 Scope
Section I - Methods for the detection of anti-oxidant
             additives
2 Detection of 2,6-di-tert-butyl-paracresol (DBPC) by
     thin layer chromatography
2.1 Summary of the method
2.2 Reagents
2.3 Equipment
2.4 Procedure
3 Detection of n-phenyl-alpha-naphtylamine (PAN) and
     n-phenyl-beta-naphtylamine (PBN) by thin layer
     chromatography
3.1 Summary of the method
3.2 Reagents
3.3 Equipment
3.4 Procedure
4 Detection of anthranilic acid in new insulating
     oils by thin layer chromatography
4.1 Summary of the method
4.2 Reagents
4.3 Equipment
4.4 Procedure
Section II - Methods for the determination of anti-
             oxidant additives
5 Determination of 2,6-di-tert-butyl-paracresol
5.1 Quantitative determination by infra-red
     spectrophotometry
5.2 Semi-quantitative determination by thin layer
     chromatography
6 Determination of n-phenyl-beta-naphtylamine by
     spectrophotometry
6.1 Summary of the method
6.2 Reagents
6.3 Equipment
6.4 Procedure
6.5 Calculation
6.6 Lower limit of detection
Figure

Procedure for detecting by thin-layer chromatography the presence of additives in unused hydrocarbon insulating oil. Also for the quantitative determination of such additives by spectrophotometry. Method intended for use where the presence of additives has been declared by the supplier.

Committee
GEL/10
DevelopmentNote
Supersedes 78/29342 DC (09/2005)
DocumentType
Standard
Pages
14
PublisherName
British Standards Institution
Status
Superseded
SupersededBy

BS 148:1998 Specification for unused and reclaimed mineral insulating oils for transformers and switchgear
BS EN 60465:1992 Specification for unused insulating mineral oils for cables with oil ducts
BS 5730:2001 Monitoring and maintenance guide for mineral insulating oils in electrical equipment
08/30167496 DC : DRAFT FEB 2008 BS 148 - RECLAIMED MINERAL INSULATING OIL FOR TRANSFORMERS AND SWITCHGEAR - SPECIFICATION
BS 148:2009 Reclaimed mineral insulating oil for transformers and switchgear. Specification
BS 148:1997 Specification for unused and reclaimed mineral insulating oils for transformers and switchgear

IEC 60590:1977 Determination of the aromatic hydrocarbon content of new mineral insulating oils
IEC 60474:1974 Test method for oxidation stability of inhibited mineral insulating oils

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