DIN EN 13925-2:2003-07
Current
The latest, up-to-date edition.
NON-DESTRUCTIVE TESTING - X-RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 2: PROCEDURES
Hardcopy , PDF
English, German
01-01-2003
Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Specimen preparation
4.1 General preparation
4.2 Block specimens
4.3 Powder specimens
4.4 Analysis of small quantities of sample
4.5 Reactive samples and non-ambient conditions
5 Data collection
5.1 General considerations
5.2 Angular range and mode of data collection
5.3 Parameters relevant to the quality of collected data
6 Data processing and analysis
6.1 Background
6.2 Peal searching
6.3 Pattern decomposition into individual line profiles
including background subtraction
6.4 Phase identification
6.5 Indexing
6.6 Lattice parameter refinement
6.7 Other types of analysis
Annex A (informative) Relationship between the XRPD standards
Annex B (informative) Example of Report Form
Annex C (informative) Scheme of a typical procedure for
XRPD measurements
Annex D (informative) Some analytical functions used for
profile fitting
Annex E (informative) Some methods for testing the internal
consistency of XRPD data
E.1 General
E.2 Figures of Merit for FWHMs and intensities
E.3 Figures of Merit for line positions and lattice
parameters
Bibliography
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