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  • EN 12457-4 : 2002

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    CHARACTERIZATION OF WASTE - LEACHING - COMPLIANCE TEST FOR LEACHING OF GRANULAR WASTE MATERIALS AND SLUDGES - ONE STAGE BATCH TEST AT A LIQUID TO SOLID RATIO OF 10 L/KG FOR MATERIALS WITH PARTICLE SIZE BELOW 10 MM (WITHOUT OR WITH SIZE REDUCTION)

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    Published date:  18-09-2002

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
      3.1 Leaching test
      3.2 Leachant
      3.3 Eluate
      3.4 Single batch leaching test
      3.5 Serial batch leaching test
      3.6 Liquid to solid ratio L/S (abbreviation: L/S)
      3.7 Liquid waste
      3.8 Sludge
      3.9 Monolithic waste
      3.10 Granular waste
      3.11 Dry matter content ratio (abbreviation: DR)
      3.12 Moisture content ratio (abbreviation MC)
      3.13 Laboratory sample
      3.14 Test sample
      3.15 Test portion
    4 Compliance test
      4.1 Principle
      4.2 Equipment and reagents
      4.3 Sampling strategy and sample preparation
    5 Procedure
      5.1 Testing conditions
      5.2 Description of the procedure
      5.3 Further preparation of the eluate for analysis
      5.4 Blank test for the verification of the leaching
           procedure
    6 Calculation
    7 Documentation and test report
      7.1 Sample preparation
      7.2 Production of eluate
      7.3 Analytical determination
      7.4 Calculations and blank test information
    8 Performance characteristics
      8.1 Objective of the validation
      8.2 Validation study
      8.3 Validation results
      8.4 Summary of the performance characteristics evaluation
    Annex A (informative) Information on the influence on the
             test results of the parameters that effect leaching
    Annex B (informative) Test for determining whether waste is
             in the liquid state
    Annex C (informative) Example of datasheet for EN 12457-4
    Annex D (informative) Process map for EN 12457-4
    Annex E (informative) Example of a specific liquid-solid
             separation procedure for soil sample
    Annex ZA (informative) National deviation A from France
    Bibliography

    Abstract - (Show below) - (Hide below)

    This part of the European Standard specifies a compliance test providing information on leaching of granular wastes and sludges under the experimental conditions specified hereafter, and particularly a liquid to solid ratio of 10 l/kg dry matter.

    General Product Information - (Show below) - (Hide below)

    Committee TC 444
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    PD CEN/TS 16660:2015 (published 2015-05) Characterization of waste. Leaching behaviour test. Determination of the reducing character and the reducing capacity
    DIN EN 14405:2017-05 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
    I.S. EN 12506:2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CL[-], CO, CR, CR (6), CU, MO, NI, NO[2-], PB, TOTAL S, SO[4][2-], V AND ZN
    I.S. EN 13370:2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, EASILY LIBERATABLE CN[-], F[-]
    I.S. EN 15863:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    BS EN 16192:2011 (published 2012-04) Characterization of waste. Analysis of eluates
    BS EN 14405:2017 (published 2017-03) Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
    14/30304804 DC : 0 BS EN 14405 - CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
    13/30286658 DC : 0 BS EN 16660 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    DIN EN 16192:2012-02 Characterization of waste - Analysis of eluates
    I.S. EN 14405:2017 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
    BS EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    10/30233988 DC : 0 BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    PD CEN/TR 16376:2012 (published 2013-01) Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
    DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    UNI EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    DIN EN 14405 E : 2017 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
    BS EN 16457:2014 (published 2014-03) Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
    04/30116791 DC : DRAFT JUL 2004 BS EN 15002 - CHARACTERISATION OF WASTE - PREPARATION OF TEST PORTIONS FROM LABORATORY SAMPLE
    FD CEN/TR 16110 : 2011 FD CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    UNE-EN 16192:2012 Characterization of waste - Analysis of eluates
    DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    S.R. CEN/TS 16660:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    S.R. CEN/TR 16110:2010 CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    I.S. EN 16192:2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    CEN/TS 16637-1 : 2014 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
    UNE-CEN/TR 16110:2011 IN Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
    BS ISO 18772 : 2008 COR 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    BS PD CEN/TS 16637-1 : 2014 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
    S.R. CEN/TR 16376:2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
    PREN 14405 : DRAFT 2014 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)
    UNI CEN/TS 16637-1 : 2014 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
    I.S. EN ISO 18772:2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
    UNE-EN 14405:2017 Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
    UNI EN 16192 : 2012 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    S.R. CEN/TS 16637-1:2014 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 1: GUIDANCE FOR THE DETERMINATION OF LEACHING TESTS AND ADDITIONAL TESTING STEPS
    DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 15863 E : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    17/30348303 DC : 0 BS EN 17087 - CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE FOR TESTING OF RELEASE AND ANALYSIS OF CONTENT
    DIN EN 15863:2015-06 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    13/30286655 DC : 0 BS EN 15863 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
    BS EN 12506:2003 (published 2003-06) Characterization of waste. Analysis of eluates. Determination of pH, As, Ba, Cd, Cl$u-, Co, Cr, Cr VI, Cu, Mo, Ni, NO2$u-, Pb, total S, SO42$u-, V and Zn
    UNE-EN 15863:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
    UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    BS EN 15002:2015 (published 2015-04) Characterization of waste. Preparation of test portions from the laboratory sample
    ISO 18772:2008 Soil quality Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
    13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    BS EN 15863:2015 (published 2015-04) Characterization of waste. Leaching behaviour test for basic characterization. Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
    BS EN 13370:2003 (published 2003-06) Characterization of waste. Analysis of eluates. Determination of Ammonium, AOX, conductivity, Hg, phenol index, TOC, easily liberatable CN$u-, F$u-
    DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 13370:2003-09 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, CN[-] EASILY LIBERATABLE, F[-]
    I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 12506:2003-09 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CI[-], CO, CR, CR(VI), CU, MO, NI, NO[2-], PB, TOTAL S, SO[4][2-], V AND ZN
    EN 12506 : 2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CL[-], CO, CR, CR (6), CU, MO, NI, NO[2][-], PB, TOTAL S, SO[4][2-], V AND ZN
    CEN/TR 16376 : 2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
    EN 14405:2017 (edition 3) Characterization of waste - Leaching behaviour test - Up-flow percolation test (under specified conditions)
    EN 15863 : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    EN 13370 : 2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, EASILY LIBERATABLE CN[-], F[-]
    CEN/TR 16110 : 2010 CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    CEN/TS 16660 : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    EN 16192 : 2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
    EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT

    Standards Referencing This Book - (Show below) - (Hide below)

    ENV 12920 : 1997 CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
    EN 12880 : 2000 CHARACTERIZATION OF SLUDGES - DETERMINATION OF DRY RESIDUE AND WATER CONTENT
    ENV 12506 : DRAFT 2000 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, CD, CR (6), CU, NI, PB, ZN, CL[-], NO[2][-], SO[4][2-]
    ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
    DIN 38414 : LATEST
    ENV 13370 : DRAFT 2001 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM - N, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, CN - EASILY LIBERATABLE, F
    EN ISO 5667-3:2012 WATER QUALITY - SAMPLING - PART 3: PRESERVATION AND HANDLING OF WATER SAMPLES (ISO 5667-3:2012)
    ISO 3696:1987 Water for analytical laboratory use Specification and test methods
    EN ISO 3696 : 1995 WATER FOR ANALYTICAL LABORATORY USE - SPECIFICATION AND TEST METHODS (ISO 3696:1987)
    NFX 31 210 : 1998
    NEN 7343 : 1995 LEACHING CHARACTERISTICS OF SOLID EARTHY AND STONY BUILDING AND WASTE MATERIALS - LEACHING TESTS - DETERMINATION OF THE LEACHING OF INORGANIC COMPONENTS FROM GRANULAR MATERIALS WITH THE COLUMN TEST
    ISO 5725-5:1998 Accuracy (trueness and precision) of measurement methods and results — Part 5: Alternative methods for the determination of the precision of a standard measurement method
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