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EN 15484:2007

Current

Current

The latest, up-to-date edition.

Ethanol as a blending component for petrol - Determination of inorganic chloride - Potentiometric method

Published date

22-08-2007

Foreword
1 Scope
2 Normative references
3 Principle
4 Reagents and materials
5 Apparatus
6 Samples and sampling
7 Calibration
   7.1 Preparation of the blank test solution
   7.2 Preparation of a 5,00 ml standard solution
   7.3 Titration
   7.4 Standardisation of 10,00 ml potassium chloride solution
   7.5 Calculation of concentration of silver nitrate solution
   7.6 Calculation of value of blank test
8 Sample analysis
   8.1 Preparation of the dry residue
   8.2 Preparation of the sample solution
   8.3 Titration
9 Calculation
10 Expression of results
11 Precision
   11.1 Repeatability, r
   11.2 Reproducibility, R
12 Test report
Annex A (informative) Measurement example
Annex B (informative) Interferences
      B.1 Introduction
      B.2 Other halogens
      B.3 Oxidizing agents
      B.4 Ammonium and iron (III) salts
      B.5 Cyanides, thiocyanates and sulphides
Bibliography

This standard specifies a potentiometric method for the determination of inorganic chloride content in ethanol from 4 mg/l to 30 mg/l. The chloride content is determined in aqueous solution after dissolution of the evaporation residue of the ethanol sample.WARNING — Use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and to determine the applicability of regulatory limitations prior to use.NOTEFor the purposes of this document, the terms “% (m/m)” and “% (V/V)” are used to represent respectively the mass fraction and the volume fraction.

Committee
CEN/TC 19
DevelopmentNote
Supersedes PREN 15484. (12/2007)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
NEN EN 15484 : 2007 Identical
I.S. EN 15484:2007 Identical
BS 2000-552(2007) : 2007 Identical
NBN EN 15484 : 2007 Identical
SN EN 15484 : 2007 Identical
BS EN 15484:2007 Identical
NS EN 15484 : 1ED 2007 Identical
PN EN 15484 : 2009 Identical
SS-EN 15484 : 2007 Identical
DIN EN 15484 E : 2007 Identical
IP 552 : 2008 Identical
UNI EN 15484 : 2008 Identical
NF EN 15484 : 2007 Identical
UNE-EN 15484:2008 Identical
DIN EN 15484:2007-11 Identical

09/30206695 DC : 0 BS EN 15376 - AUTOMOTIVE FUELS - ETHANOL AS A BLENDING COMPONENT FOR PETROL - REQUIREMENTS AND TEST METHODS

ISO 3170:2004 Petroleum liquids — Manual sampling
ISO 1042:1998 Laboratory glassware One-mark volumetric flasks
ISO 6227:1982 Chemical products for industrial use General method for determination of chloride ions Potentiometric method
EN ISO 1042 : 1999 LABORATORY GLASSWARE - ONE-MARK VOLUMETRIC FLASKS
ISO 4259:2006 Petroleum products Determination and application of precision data in relation to methods of test
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN ISO 3170:2004 Petroleum liquids - Manual sampling (ISO 3170:2004)
EN ISO 4259:2006 Petroleum products - Determination and application of precision data in relation to methods of test (ISO 4259:2006)

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