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  • EN 15934 : 2012

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    SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - CALCULATION OF DRY MATTER FRACTION AFTER DETERMINATION OF DRY RESIDUE OR WATER CONTENT

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    Language(s): 

    Published date:  22-08-2012

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Sample preparation
    6 Method A - Drying at 105 degrees C
    7 Method B - Direct Karl-Fischer-titration
       (volumetric/coulometric detection)
    8 Calculation of dry matter fraction
    9 Precision
    10 Test report
    Annex A (informative) - Repeatability and reproducibility
    Annex B (informative) - Azeotropic distillation with toluene
    Annex C (informative) - Summary of general requirements
            and recommendations

    Abstract - (Show below) - (Hide below)

    This European Standard specifies methods for the calculation of the dry matter of sludge, treated biowaste, soil and waste for which the results of performed analysis are to be calculated to the dry matter basis.

    General Product Information - (Show below) - (Hide below)

    Committee TC 444
    Development Note Supersedes PREN 15934. (09/2012)
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Current

    Standards Referenced By This Book - (Show below) - (Hide below)

    ISO 13913:2014 Soil quality Determination of selected phthalates using capillary gas chromatography with mass spectrometric detection (GC/MS)
    17/30362321 DC : 0 BS EN ISO 23161 - SOIL QUALITY - DETERMINATION OF SELECTED ORGANOTIN COMPOUNDS - GAS-CHROMATOGRAPHIC METHOD
    BS EN 16179 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
    BS EN 15936:2012 (published 2012-09) Sludge, treated biowaste, soil and waste. Determination of total organic carbon (TOC) by dry combustion
    BS EN 16168 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
    DIN EN 15935 E : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
    BS EN 16175-2:2016 Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS)
    ISO 18187:2016 Soil quality Contact test for solid samples using the dehydrogenase activity of Arthrobacter globiformis
    BS EN 16166:2012 (published 2012-09) Sludge, treated biowaste and soil. Determination of adsorbable organically bound halogens (AOX)
    VDI 3957-2 : 2016 BIOLOGICAL MEASURING TECHNIQUES FOR THE DETERMINATION AND ASSESSMENT OF EFFECTS OF AIR POLLUTANTS ON PLANTS (BIOMONITORING) - METHOD OF THE STANDARDISED GRASS EXPOSURE
    BS EN 15935:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
    UNI EN 15936 : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
    UNI CEN/TS 16172 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
    BS ISO 16729 : 2013 SOIL QUALITY - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
    DIN EN 16169:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
    BS ISO 18187 : 2016 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS
    UNI EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    S.R. CEN/TS 16170:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    UNI CEN/TS 16183 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC-MS)
    BS EN 16169 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
    UNI EN 16173 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
    S.R. CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
    UNI CEN/TS 16170 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    DIN EN 16179:2012-11 Sludge, treated biowaste and soil - Guidance for sample pretreatment
    BS PD CEN/TR 16193 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETECTION AND ENUMERATION OF ESCHERICHIA COLI
    BS EN 16173:2012 (published 2012-09) Sludge, treated biowaste and soil. Digestion of nitric acid soluble fractions of elements
    DIN EN 16166:2012-11 Sludge, treated biowaste and soil - Determination of adsorbable organically bound halogens (AOX)
    BS ISO 13913 : 2014 SOIL QUALITY - DETERMINATION OF SELECTED PHTHALATES USING CAPILLARY GAS CHROMATOGRAPHY WITH MASS SPECTROMETRIC DETECTION (GC/MS)
    UNI EN 15935 : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
    S.R. CEN/TS 16175-2:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
    DIN EN 16168:2012-11 Sludge, treated biowaste and soil - Determination of total nitrogen using dry combustion method; German version EN 16168:2012
    UNI CEN/TS 16189 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF LINEAR ALKYLBENZENE SULFONATES (LAS) BY HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC) WITH FLUORESCENCE DETECTION (FLD) OR MASS SELECTIVE DETECTION (MS)
    UNI CEN/TS 16182 : 2012 SLUDGE TREATED BIOWASTE AND SOIL - DETERMINATION OF NONYLPHENOLS (NP) AND NONYLPHENOL-MONO- AND DIETHOXYLATES USING GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GCMS)
    DIN EN 16173:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
    UNI EN 16169 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
    DIN EN 15936 E : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
    I.S. EN 16179:2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
    S.R. CEN/TR 16193:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETECTION AND ENUMERATION OF ESCHERICHIA COLI
    I.S. EN 15936:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
    EN ISO 18187 : 2018 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS (ISO 18187:2016)
    I.S. EN 16170:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    I.S. EN 16167:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRONCAPTURE DETECTION (GC-ECD)
    I.S. EN 16166:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX)
    I.S. EN 16173:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
    I.S. EN ISO 18187:2018 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS (ISO 18187:2016)
    I.S. EN 16175-2:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
    S.R. CEN/TS 16175-1:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
    I.S. EN 16169:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
    I.S. EN 16171:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    I.S. EN 16168:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
    DIN EN 16167:2012-11 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    EN 16167 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    17/30364002 DC : 0 BS EN 16167 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    I.S. EN 16175-1:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
    17/30363999 DC : 0 BS EN 16190 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    UNE-EN 16179:2013 Sludge, treated biowaste and soil - Guidance for sample pretreatment
    UNI EN 16179 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
    UNI CEN/TS 16171 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    CEN/TR 16193 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETECTION AND ENUMERATION OF ESCHERICHIA COLI
    UNI EN 16168 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
    ISO 16729:2013 Soil quality Digestion of nitric acid soluble fractions of elements
    S.R. CEN/TS 16171:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    I.S. EN 15935:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
    EN 15935 : 2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF LOSS ON IGNITION
    PREN 16190 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF DIOXINS AND FURANS AND DIOXIN-LIKE POLYCHLORINATED BIPHENYLS BY GAS CHROMATOGRAPHY WITH HIGH RESOLUTION MASS SELECTIVE DETECTION (HR GC-MS)
    BS EN ISO 18187 : 2018 SOIL QUALITY - CONTACT TEST FOR SOLID SAMPLES USING THE DEHYDROGENASE ACTIVITY OF ARTHROBACTER GLOBIFORMIS
    PREN 16167 : DRAFT 2017 SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCHLORINATED BIPHENYLS (PCB) BY GAS CHROMATOGRAPHY WITH MASS SELECTIVE DETECTION (GC-MS) AND GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION (GC-ECD)
    17/30364005 DC : 0 BS EN 16181 - SOIL, TREATED BIOWASTE AND SLUDGE - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    S.R. CEN/TS 16181:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    CEN/TS 16171 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
    CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
    EN 16175-2:2016 (edition 2) Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
    DIN EN 15935:2012-11 Sludge, treated biowaste, soil and waste - Determination of loss on ignition; German version EN 15935:2012
    CEN/TS 16175-1 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
    DIN EN 15936:2012-11 Sludge, treated biowaste, soil and waste - Determination of total organic carbon (TOC) by dry combustion
    CEN/TS 16181 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)
    CEN/TS 16175-2 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
    UNI EN 16166 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX)
    CEN/TS 16170 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
    EN 16166 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ADSORBABLE ORGANICALLY BOUND HALOGENS (AOX)
    EN 16169 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF KJELDAHL NITROGEN
    EN 16179 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
    EN 16168 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF TOTAL NITROGEN USING DRY COMBUSTION METHOD
    EN 16173 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DIGESTION OF NITRIC ACID SOLUBLE FRACTIONS OF ELEMENTS
    EN 15936:2012 SLUDGE, TREATED BIOWASTE, SOIL AND WASTE - DETERMINATION OF TOTAL ORGANIC CARBON (TOC) BY DRY COMBUSTION
    UNI CEN/TS 16181 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF POLYCYCLIC AROMATIC HYDROCARBONS (PAH) BY GAS CHROMATOGRAPHY (GC) AND HIGH PERFORMANCE LIQUID CHROMATOGRAPHY (HPLC)

    Standards Referencing This Book - (Show below) - (Hide below)

    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN 16179 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - GUIDANCE FOR SAMPLE PRETREATMENT
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