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EN 16173:2012

Current

Current

The latest, up-to-date edition.

Sludge, treated biowaste and soil - Digestion of nitric acid soluble fractions of elements

Published date

22-08-2012

Foreword
Introduction
1 Scope
2 Normative references
3 Principle
4 Interferences and sources of errors
5 Reagents
6 Apparatus
7 Digestion procedure
8 Test report
Annex A (informative) - Repeatability and
        reproducibility data
Bibliography

This European Standard specifies a method for microwave digestion of sludge, treated biowaste and soil using nitric acid.This method is applicable for microwave-assisted nitric acid digestion of sludge, treated biowaste and soils for the following elements: Aluminium (Al), antimony (Sb), arsenic (As), barium (Ba), beryllium (Be), bismuth (Bi), boron (B), cadmium (Cd), calcium (Ca), cerium (Ce), cesium (Cs), chromium (Cr), cobalt (Co), copper (Cu), dysprosium (Dy), erbium (Er), europium (Eu), gadolinium (Gd), gallium (Ga), germanium (Ge), gold (Au), hafnium (Hf), holmium (Ho), indium (In), iridium (Ir), iron (Fe), lanthanum (La), lead (Pb), lithium (Li), lutetium (Lu), magnesium (Mg), manganese (Mn), mercury (Hg), molybdenum (Mo), neodymium (Nd), nickel (Ni), palladium (Pd), phosphorus (P), platinum (Pt), potassium (K), praseodymium (Pr), rubidium (Rb), rhenium (Re), rhodium (Rh), ruthenium (Ru), samarium (Sm), scandium (Sc), selenium (Se), silicon (Si), sodium (Na), strontium (Sr), sulphur (S), tellurium (Te), terbium (Tb), thallium (Tl), thorium (Th), thulium (Tm), tin (Sn), titanium (Ti), tungsten (W), uranium (U), vanadium (V), ytterbium (Yb), yttrium (Y), zinc (Zn), and zirconium (Zr).This European Standard may also be applicable for the digestion of other elements. Digestion with nitric acid will not necessarily accomplish total decomposition of the sample. The extracted analyte concentrations may not necessarily reflect the total content in the sample.

Committee
CEN/TC 444
DevelopmentNote
Supersedes PREN 16173. (09/2012)
DocumentType
Standard
PublisherName
Comite Europeen de Normalisation
Status
Current

Standards Relationship
BS EN 16173:2012 Identical
NS EN 16173 : 2012 Identical
NEN EN 16173 : 2012 Identical
DIN EN 16173:2012-11 Identical
UNI EN 16173 : 2012 Identical
I.S. EN 16173:2012 Identical
UNE-EN 16173:2012 Identical
NF EN 16173 : 2012 Identical
NBN EN 16173 : 2012 Identical
SN EN 16173:2012 Identical
PN EN 16173 : 2012 Identical

S.R. CEN/TS 16171:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
S.R. CEN/TS 16170:2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
PD ISO/TS 16965:2013 Soil quality. Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
ISO/TS 16965:2013 Soil quality Determination of trace elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/TS 16171:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma mass spectrometry (ICP-MS)
CEN/TS 16172:2013 Sludge, treated biowaste and soil - Determination of elements using graphite furnace atomic absorption spectrometry (GF-AAS)
EN 16175-2:2016 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
CEN/TS 16175-1:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 1: Cold-vapour atomic absorption spectrometry (CV-AAS)
UNI CEN/TS 16170 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
BS EN 16175-2:2016 Sludge, treated biowaste and soil. Determination of mercury Cold-vapour atomic fluorescence spectrometry (CV-AFS)
UNI CEN/TS 16172 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
UNI CEN/TS 16188 : 2012 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS IN AQUA REGIA AND NITRIC ACID DIGESTS - FLAME ATOMIC ABSORPTION SPECTROMETRY METHOD (FAAS)
I.S. EN 16175-1:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
UNI CEN/TS 16171 : 2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
S.R. CEN/TS 16172:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY (GF-AAS)
S.R. CEN/TS 16175-2:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
I.S. EN 16171:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS)
I.S. EN 16170:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF ELEMENTS USING INDUCTIVELY COUPLED PLASMA OPTICAL EMISSION SPECTROMETRY (ICP-OES)
I.S. EN 16175-2:2016 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 2: COLD-VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY (CV-AFS)
S.R. CEN/TS 16175-1:2013 SLUDGE, TREATED BIOWASTE AND SOIL - DETERMINATION OF MERCURY - PART 1: COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY (CV-AAS)
CEN/TS 16175-2:2013 Sludge, treated biowaste and soil - Determination of mercury - Part 2: Cold-vapour atomic fluorescence spectrometry (CV-AFS)
CEN/TS 16170:2012 Sludge, treated biowaste and soil - Determination of elements using inductively coupled plasma optical emission spectrometry (ICP-OES)

EN ISO 15587-2 : 2002 WATER QUALITY - DIGESTION FOR THE DETERMINATION OF SELECTED ELEMENTS IN WATER - NITRIC ACID DIGESTION
ISO 15587-2:2002 Water quality — Digestion for the determination of selected elements in water — Part 2: Nitric acid digestion
ISO 11074:2015 Soil quality — Vocabulary
EN 14888:2005 Fertilizers and liming materials - Determination of cadmium content
ISO 5725-2:1994 Accuracy (trueness and precision) of measurement methods and results Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method
ISO 3696:1987 Water for analytical laboratory use — Specification and test methods
EN ISO 3696:1995 Water for analytical laboratory use - Specification and test methods (ISO 3696:1987)
EN 15934:2012 Sludge, treated biowaste, soil and waste - Calculation of dry matter fraction after determination of dry residue or water content
EN 16179:2012 Sludge, treated biowaste and soil - Guidance for sample pretreatment

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