• ASTM D 7458 : 2014

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    Standard Test Method for Determination of Beryllium in Soil, Rock, Sediment, and Fly Ash Using Ammonium Bifluoride Extraction and Fluorescence Detection

    Available format(s):  Hardcopy, PDF

    Superseded date:  02-09-2021

    Language(s):  English

    Published date:  02-09-2021

    Publisher:  American Society for Testing and Materials

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    1.1This test method is intended for use in the determination of beryllium in samples of soil, rock, sediment, and fly ash. This test method can be used for purposes such as environmental remediation projects where beryllium is a contaminant of concern. It is also useful for characterization of levels of beryllium in soil at sites where beryllium is in mining or manufacturing applications, and for determination of background levels of beryllium in soil.

    1.2This test method assumes that samples of soil, rock, sediment, or fly ash are collected using appropriate and applicable ASTM International standard practices.

    1.3This test method includes a procedure for extraction (dissolution) of beryllium in dilute ammonium bifluoride, followed by analysis of aliquots of the extract solution using a beryllium-specific fluorescent dye.

    1.4No detailed operating instructions are provided because of differences among various makes and models of suitable fluorometric instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.

    1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

    1.6All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.

    1.6.1The procedures used to specify how data are collected/recorded, or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.

    1.7This test method contains notes that are explanatory and not part of mandatory requirements of the standard.

    1.8This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards associated with performance of this test method are described in Section 9.

    General Product Information - (Show below) - (Hide below)

    Committee D 22
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Superseded
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM D 7202 : 2015 Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM D 4840 : 1999 : R2018 : EDT 1 Standard Guide for Sample Chain-of-Custody Procedures
    ASTM D 5730 : 2002 Standard Guide for Site Characterization for Environmental Purposes With Emphasis on Soil, Rock, the Vadose Zone and Ground Water
    ASTM D 653 : 2007 Standard Terminology Relating to Soil, Rock, and Contained Fluids
    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM D 4840 : 1999 Standard Guide for Sampling Chain-of-Custody Procedures
    ASTM D 3740 : 2012 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 5730 : 1998 Standard Guide for Site Characterization for Environmental Purposes With Emphasis on Soil, Rock, the Vadose Zone and Ground Water
    ASTM D 3740 : 2019 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 3740 : 2004 : REV A : EDT 1 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 3740 : 2008 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM D 6026 : 2013 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 7202 : 2014 : EDT 1 Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
    ASTM D 6026 : 2006 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 7202 : 2006 Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Fluorescence Detection
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 3740 : 1999 : REV C Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 7202 : 2014 Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
    ASTM D 7202 : 2011 Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Optical Fluorescence Detection
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM D 653 : 2020 : EDT 1 Standard Terminology Relating to Soil, Rock, and Contained Fluids
    ASTM D 7202 : 2015 Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection
    ASTM D 6026 : 1999 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 3740 : 2011 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6026 : 2001 : EDT 1 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM D 3740 : 2010 Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 653 : 2021 : REV A Standard Terminology Relating to Soil, Rock, and Contained Fluids
    ASTM D 6026 : 1996 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 3740 : 2004 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 3740 : 2001 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 653 : 2021 Standard Terminology Relating to Soil, Rock, and Contained Fluids
    ASTM D 653 : 2021 : REV B Standard Terminology Relating to Soil, Rock, and Contained Fluids
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 6026 : 1996 : EDT 1 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 3740 : 2012 : REV A Standard Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 3740 : 2003 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM D 6026 : 2021 Standard Practice for Using Significant Digits and Data Records in Geotechnical Data
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM D 6026 : 2001 Standard Practice for Using Significant Digits in Geotechnical Data
    ASTM D 7202 : 2005 Standard Test Method for Determination of Beryllium in the Workplace Using Field-Based Extraction and Fluorescence Detection
    ASTM D 5730 : 2004 Standard Guide for Site Characterization for Environmental Purposes With Emphasis on Soil, Rock, the Vadose Zone and Groundwater (Withdrawn 2013)
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM D 3740 : 2004 Standard Practice for Minimum Requirements for Agencies Engaged in the Testing and/or Inspection of Soil and Rock as Used in Engineering Design and Construction
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