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ASTM D 128 : 1998 : R2019

Current

Current

The latest, up-to-date edition.

Standard Test Methods for Analysis of Lubricating Grease

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

31-07-2019

1.1These test methods for analysis cover greases of the conventional type, which consist essentially of petroleum oil and soap. The constituents that can be determined are soap, unsaponifiable matter (petroleum oil, and so forth), water, free alkalinity, free fatty acid, fat, glycerin, and insolubles.

Note 1:Any of the test methods described herein are best used by an experienced grease analyst who may also be able to make appropriate adaptations of the techniques as occasion requires.

1.2A supplementary test method is provided in Appendix X1. This test method is intended primarily for application to greases containing thickeners that are essentially insoluble in n-hexane, and to greases that cannot be analyzed by conventional methods because of the presence of such constituents as nonpetroleum fluids or nonsoap-type thickeners, or both. In some cases, these constituents can react with strong acid or alkaline solutions.

1.3These test methods appear in the following order:

Sections

Ash Determination

7 – 11

Insolubles, Soap, Fat, Petroleum Oil,
 and Unsaponifiable Matter

12 – 20

Free Alkali and Free Acid

21 – 23

Water

24

Glycerin (Quantitative)

25 – 29

1.4The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.5This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.

1.6This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

Committee
D 02
DocumentType
Test Method
Pages
11
PublisherName
American Society for Testing and Materials
Status
Current
Supersedes

ASTM D 473 : 1981 : R1995 : EDT 2 Standard Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method
ASTM D 217 : 2021 Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 1078 : 1999 Standard Test Method for Distillation Range of Volatile Organic Liquids
ASTM D 473 : 2007 : R2017 : EDT 1 Standard Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method
ASTM D 217 : 2021 : REV A Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 473 : 2022 Standard Test Method for Sediment in Crude Oils and Fuel Oils by the Extraction Method
ASTM D 445 : 2021 : EDT 2 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 804 : 2012 : R2017 Standard Terminology Relating to Pine Chemicals, Including Tall Oil and Related Products
ASTM D 445 : 2017 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 156 : 2015 Standard Test Method for Saybolt Color of Petroleum Products (Saybolt Chromometer Method)
ASTM D 445 : 1988 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity)
ASTM D 217 : 2019 : REV B Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 95 : 2013 : R2018 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
ASTM D 445 : 2019 : REV A Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 217 : 1997 Standard Test Methods for Cone Penetration of Lubricating Grease
ASTM D 1353 : 1983 : EDT 1 Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
ASTM D 804 : 2012 : R2022 Standard Terminology Relating to Pine Chemicals, Including Tall Oil and Related Products
ASTM D 445 : 2019 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 156 : 2023 Standard Test Method for Saybolt Color of Petroleum Products (Saybolt Chromometer Method)
ASTM D 445 : 2001 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity)
ASTM D 445 : 2024 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 445 : 2021 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 1193 : 1970 Standard Specification For Reagent Water
ASTM D 445 : 2018 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 1353 : 2013 : R2021 Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
ASTM D 445 : 2021 : EDT 1 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)
ASTM D 1353 : 2013 Standard Test Method for Nonvolatile Matter in Volatile Solvents for Use in Paint, Varnish, Lacquer, and Related Products
ASTM D 95 : 2023 Standard Test Method for Water in Petroleum Products and Bituminous Materials by Distillation
ASTM D 445 : 2023 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity)

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