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  • ASTM E 2823 : 2017

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    Standard Test Method for Analysis of Nickel Alloys by Inductively Coupled Plasma Mass Spectrometry (Performance-Based)

    Available format(s):  Hardcopy, PDF

    Language(s):  English

    Published date:  01-01-2017

    Publisher:  American Society for Testing and Materials

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    1.1This test method describes the inductively coupled plasma mass spectrometric analysis of nickel and nickel allys, as specified by Committee B02, and having chemical compositions within the following limits:

    Element

    Application Range (Mass Fraction %)

    Aluminum

    0. 01–6.00

    Boron

    0. 01–0.10

    Carbon

    0. 01–0.15

    Chromium

    0. 01–33.00

    Copper

    0.01–35.00

    Cobalt

    0. 01–20.00

    Iron

    0.05–50.00

    Magnesium

    0. 01–0.020

    Molybdenum

    0. 01–30.0

    Niobium

    0. 01–6.0

    Nickel

    25.00–100.0

    Phosphorous

    0.001–0.025

    Silicon

    0.01–1.50

    Sulfur

    0.0001–0.01

    Titanium

    0.0001–6.0

    Tungsten

    0.01–5.0

    Vanadium

    0.0005–1.0

    1.2The following elements may be determined using this method.

    Element

    Quantification Range (μg/g)

    Antimony

    0.5–50

    Bismuth

    0.1–11

    Gallium

    2.9–54

    Lead

    0.4–21

    Silver

    1–35

    Tin

    2.2–97

    Thallium

    0.5–3.0

    1.3This method has only been interlaboratory tested for the elements and ranges specified. It may be possible to extend this method to other elements or different composition ranges provided that method validation that includes evaluation of method sensitivity, precision, and bias as described in this document is performed. Additionally, the validation study must evaluate the acceptability of sample preparation methodology using reference materials and/or spike recoveries. The user is cautioned to carefully evaluate the validation data as to the intended purpose of the analytical results. Guide E2857 provides additional guidance on method validation.

    1.4This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific safety hazard statements are given in Section 9.

    General Product Information - (Show below) - (Hide below)

    Committee E 01
    Document Type Test Method
    Publisher American Society for Testing and Materials
    Status Current
    Supersedes

    Standards Referenced By This Book - (Show below) - (Hide below)

    ASTM E 1473 : 2016 Standard Test Methods for Chemical Analysis of Nickel, Cobalt and High-Temperature Alloys

    Standards Referencing This Book - (Show below) - (Hide below)

    ASTM E 2027 : 2017 : EDT 1 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E 177 : 1990 : REV A : R1996 Standard Practice for Use of the Terms Precision and Bias in ASTM Test Methods
    ASTM E 1479 : 2016 Standard Practice for Describing and Specifying Inductively Coupled Plasma Atomic Emission Spectrometers
    ASTM E 29 : 2013 : R2019 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM E 1479 : 1999 : R2005 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
    ASTM E 2857 : 2021 Standard Guide for Validating Analytical Methods
    ASTM E 29 : 2002 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
    ASTM D 1193 : 1977 : R1983 : EDT 1 Standard Specification for Reagent Water
    ASTM E 135 : 2021 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 1329 : 2000 : R2005 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
    ASTM E 691 : 2020 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 2165 : 2001 Standard Practice for Establishing an Uncertainty Budget for the Chemical Analysis of Metals, Ores, and Related Materials (Withdrawn 2007)
    ASTM E 2027 : 2009 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E 2027 : 2017 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E 691 : 2019 : EDT 1 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 135 : 2003 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM D 1193 : 2006 : R2011 Standard Specification for Reagent Water
    ASTM E 1601 : 2019 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 1601 : 1998 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 2972 : 2015 Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
    ASTM E 1601 : 2010 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 1329 : 2010 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis (Withdrawn 2019)
    ASTM E 1479 : 1999 : R2011 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
    ASTM E 1329 : 2000 Standard Practice for Verification and Use of Control Charts in Spectrochemical Analysis
    ASTM E 691 : 2009 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM D 1193 : 1991 Standard Specification for Reagent Water
    ASTM E 135 : 2002 : REV A Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 1601 : 2012 Standard Practice for Conducting an Interlaboratory Study to Evaluate the Performance of an Analytical Method
    ASTM E 2857 : 2011 : R2021 : EDT 1 Standard Guide for Validating Analytical Methods
    ASTM E 691 : 2021 Standard Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
    ASTM E 2857 : 2011 : R2016 Standard Guide for Validating Analytical Methods
    ASTM E 2027 : 1999 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E2972 : 2015(2019) Standard Guide for Production, Testing, and Value Assignment of In-House Reference Materials for Metals, Ores, and Other Related Materials
    ASTM E 2027 : 2005 Standard Practice for Conducting Proficiency Tests in the Chemical Analysis of Metals, Ores, and Related Materials
    ASTM E 135 : 2021 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 135 : 2003 Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM E 135 : 2003 : REV C Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM D 1193 : 1970 Standard Specification For Reagent Water
    ASTM E 2857 : 2011 Standard Guide for Validating Analytical Methods
    ASTM D 1193 : 2006 Standard Specification for Reagent Water
    ASTM E 50 : 1982 : R1986 Standard Practices for Apparatus, Reagents, and Safety Precautions for Chemical Analysis of Metals
    ASTM D 1193 : 1999 Standard Specification for Reagent Water
    ASTM E 135 : 2020 : REV B Standard Terminology Relating to Analytical Chemistry for Metals, Ores, and Related Materials
    ASTM D 1193 : 2006 : R2018 Standard Specification for Reagent Water
    ASTM E 1479 : 1999 Standard Practice for Describing and Specifying Inductively-Coupled Plasma Atomic Emission Spectrometers
    ASTM E 29 : 2022 Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
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