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  • CEN/TS 14405 : 2004

    Superseded A superseded Standard is one, which is fully replaced by another Standard, which is a new edition of the same Standard.
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    CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TESTS - UP-FLOW PERCOLATION TEST (UNDER SPECIFIED CONDITIONS)

    Available format(s): 

    Superseded date:  01-03-2017

    Language(s): 

    Published date:  12-01-2013

    Publisher:  Comite Europeen de Normalisation

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    Table of Contents - (Show below) - (Hide below)

    Foreword
    Introduction
    1 Scope
    2 Normative references
    3 Terms and definitions
    4 Principle
    5 Equipment and reagents
       5.1 General
    6 Sample pre-treatment
       6.1 General
       6.2 Sample preparation
       6.3 Test portion
       6.4 Determination of dry residue
    7 Procedure
       7.1 Temperature
       7.2 Preparation
       7.3 Packing of the column
       7.4 Start-up of the test
       7.5 Collection of additional eluate fractions
       7.6 Further preparation of the eluates for analysis
       7.7 Blank test
    8 Calculations
    9 Test report
    10 Test performance
    Annex A (informative) Illustration of the column and
                          accompanying equipment
    Annex B (informative) Suggestions for packing the column,
                          water saturation and establishment
                          and checking of equilibrium
                          conditions
       B.1 General
       B.2 Guidelines on column filling and packing
       B.3 Water saturation
       B.4 Equilibration and checking of equilibrium conditions
    Annex C (informative) Background for the choices made in
                          developing this percolation test
       C.1 Introduction
       C.2 Particle size/particle size distribution
       C.3 Column dimensions
       C.4 Flow mode (up-flow/down-flow)
       C.5 Flow rate of the leachant
       C.6 L/S ratio and eluate fractions collected/duration of
           the test
       C.7 Nature of the leachant
       C.8 Temperature
       C.9 Beneficial use of the test results
    Bibliography

    Abstract - (Show below) - (Hide below)

    Applies to determine the leaching behaviour of inorganic constituents from granular waste (without or with size reduction).

    General Product Information - (Show below) - (Hide below)

    Committee TC 292
    Document Type Standard
    Publisher Comite Europeen de Normalisation
    Status Superseded
    Superseded By

    Standards Referenced By This Book - (Show below) - (Hide below)

    PD CEN/TS 15864:2012 (published 2012-07) Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with continuous leachant renewal under conditions relevant for specified scenario(s)
    PD CEN/TS 16637-3:2016 (published 2016-06) Construction products. Assessment of release of dangerous substances Horizontal up-flow percolation test
    PD CEN/TS 16660:2015 (published 2015-05) Characterization of waste. Leaching behaviour test. Determination of the reducing character and the reducing capacity
    I.S. EN 15863:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    BS EN 16192:2011 (published 2012-04) Characterization of waste. Analysis of eluates
    13/30286658 DC : 0 BS EN 16660 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    DIN EN 16192:2012-02 Characterization of waste - Analysis of eluates
    DIN EN ISO 18772 E : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
    BS EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    PD CEN/TR 16098:2010 (published 2010-12) Construction products. Assessment of release of dangerous substances. Concept of horizontal testing procedures in support of requirements under the CPD
    UNI EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    10/30233988 DC : 0 BS EN 16192 - CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    PD CEN/TR 16376:2012 (published 2013-01) Characterization of waste. Overall guidance document for characterization of waste from the extractive industries
    DIN EN 16457 E : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    12/30263896 DC : 0 BS EN 16457 - CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    UNE-EN 16457:2014 Characterization of waste - Framework for the preparation and application of a testing programme - Objectives, planning and report
    UNI EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    DIN EN ISO 18772:2014-07 Soil quality - Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials (ISO 18772:2008)
    BS EN 16457:2014 (published 2014-03) Characterization of waste. Framework for the preparation and application of a testing programme. Objectives, planning and report
    FD CEN/TR 16110 : 2011 FD CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    UNE-EN 16192:2012 Characterization of waste - Analysis of eluates
    DIN EN 16457:2014-07 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    S.R. CEN/TS 16660:2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    S.R. CEN/TR 16110:2010 CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    I.S. EN 16192:2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    S.R. CEN ISO TS 21268-3:2009 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 3: UP-FLOW PERCOLATION TEST
    I.S. EN 16457:2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT
    S.R. CEN/TR 16098:2010 CONSTRUCTION PRODUCTS: ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - CONCEPT OF HORIZONTAL TESTING PROCEDURES IN SUPPORT OF REQUIREMENTS UNDER THE CPD
    S.R. CEN/TS 16637-3:2016 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 3: HORIZONTAL UP-FLOW PERCOLATION TEST
    UNE-CEN/TR 16110:2011 IN Characterization of waste - Guidance on the use of ecotoxicity tests applied to waste
    BS ISO 18772 : 2008 COR 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS
    S.R. CEN/TR 16376:2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
    I.S. EN ISO 18772:2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
    UNI CEN ISO/TS 21268-3 : 2010 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 3: UP-FLOW PERCOLATION TEST
    UNI EN 16192 : 2012 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    S.R. CEN/TS 15864:2015 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH CONTINUOUS LEACHANT RENEWAL UNDER CONDITIONS RELEVANT FOR SPECIFIED SCENARIO(S)
    DIN EN 15002 E : 2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    DIN EN 15863 E : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    DIN EN 15863:2015-06 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    13/30286655 DC : 0 BS EN 15863 - CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
    PD CEN/TS 15862:2012 (published 2012-07) Characterisation of waste. Compliance leaching test. One stage batch leaching test for monoliths at fixed liquid to surface area ratio (L/A) for test portions with fixed minimum dimensions
    PD CEN/TS 15863:2012 (published 2012-07) Characterisation of waste. Leaching behaviour test for basic characterisation. Dynamic monolithic leaching test with periodic leachant renewal, under fixed test conditions
    ISO/TS 21268-3:2007 Soil quality Leaching procedures for subsequent chemical and ecotoxicological testing of soil and soil materials Part 3: Up-flow percolation test
    UNE-EN 15863:2015 Characterization of waste - Leaching behaviour test for basic characterization - Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
    UNE-EN 15002:2015 Characterization of waste - Preparation of test portions from the laboratory sample
    BS EN 15002:2015 (published 2015-04) Characterization of waste. Preparation of test portions from the laboratory sample
    ISO 18772:2008 Soil quality Guidance on leaching procedures for subsequent chemical and ecotoxicological testing of soils and soil materials
    13/30291099 DC : 0 BS EN 15002 - CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    BS EN 15863:2015 (published 2015-04) Characterization of waste. Leaching behaviour test for basic characterization. Dynamic monolithic leaching test with periodic leachant renewal, under fixed conditions
    DIN EN 15002:2015-07 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    S.R. CEN/TS 15863:2012 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERISATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
    I.S. EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    S.R. CEN/TS 15862:2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
    CEN/TS 15862 : 2012 CHARACTERISATION OF WASTE - COMPLIANCE LEACHING TEST - ONE STAGE BATCH LEACHING TEST FOR MONOLITHS AT FIXED LIQUID TO SURFACE AREA RATIO (L/A) FOR TEST PORTIONS WITH FIXED MINIMUM DIMENSIONS
    CEN/TR 16376 : 2012 CHARACTERIZATION OF WASTE - OVERALL GUIDANCE DOCUMENT FOR CHARACTERIZATION OF WASTE FROM THE EXTRACTIVE INDUSTRIES
    CEN/TS 16637-3 : 2016 CONSTRUCTION PRODUCTS - ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - PART 3: HORIZONTAL UP-FLOW PERCOLATION TEST
    EN 15863 : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED CONDITIONS
    CEN/TR 16098 : 2010 CONSTRUCTION PRODUCTS: ASSESSMENT OF RELEASE OF DANGEROUS SUBSTANCES - CONCEPT OF HORIZONTAL TESTING PROCEDURES IN SUPPORT OF REQUIREMENTS UNDER THE CPD
    CEN/TS 15864:2015 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERIZATION - DYNAMIC MONOLITHIC LEACHING TEST WITH CONTINUOUS LEACHANT RENEWAL UNDER CONDITIONS RELEVANT FOR SPECIFIED SCENARIO(S)
    CEN/TR 16110 : 2010 CHARACTERIZATION OF WASTE - GUIDANCE ON THE USE OF ECOTOXICITY TESTS APPLIED TO WASTE
    CEN/TS 16660 : 2015 CHARACTERIZATION OF WASTE - LEACHING BEHAVIOUR TEST - DETERMINATION OF THE REDUCING CHARACTER AND THE REDUCING CAPACITY
    CEN ISO/TS 21268-3 : 2009 SOIL QUALITY - LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOIL AND SOIL MATERIALS - PART 3: UP-FLOW PERCOLATION TEST
    EN 16192 : 2011 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES
    CEN/TS 15863 : 2012 CHARACTERISATION OF WASTE - LEACHING BEHAVIOUR TEST FOR BASIC CHARACTERISATION - DYNAMIC MONOLITHIC LEACHING TEST WITH PERIODIC LEACHANT RENEWAL, UNDER FIXED TEST CONDITIONS
    EN 15002:2015 CHARACTERIZATION OF WASTE - PREPARATION OF TEST PORTIONS FROM THE LABORATORY SAMPLE
    EN ISO 18772 : 2014 SOIL QUALITY - GUIDANCE ON LEACHING PROCEDURES FOR SUBSEQUENT CHEMICAL AND ECOTOXICOLOGICAL TESTING OF SOILS AND SOIL MATERIALS (ISO 18772:2008)
    EN 16457 : 2014 CHARACTERIZATION OF WASTE - FRAMEWORK FOR THE PREPARATION AND APPLICATION OF A TESTING PROGRAMME - OBJECTIVES, PLANNING AND REPORT

    Standards Referencing This Book - (Show below) - (Hide below)

    PREN 14346 : DRAFT 2004 CHARACTERIZATION OF WASTE - CALCULATION OF DRY MATTER BY DETERMINATION OF DRY RESIDUE AND WATER CONTENT
    ENV 12920 : 1997 CHARACTERIZATION OF WASTE - METHODOLOGY FOR THE DETERMINATION OF THE LEACHING BEHAVIOUR OF WASTE UNDER SPECIFIED CONDITIONS
    ISO 11464:2006 Soil quality Pretreatment of samples for physico-chemical analysis
    ISO 5667-3:2012 Water quality Sampling Part 3: Preservation and handling of water samples
    EN 13370 : 2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF AMMONIUM, AOX, CONDUCTIVITY, HG, PHENOL INDEX, TOC, EASILY LIBERATABLE CN[-], F[-]
    EN ISO 5667-3:2012 WATER QUALITY - SAMPLING - PART 3: PRESERVATION AND HANDLING OF WATER SAMPLES (ISO 5667-3:2012)
    EN 12506 : 2003 CHARACTERIZATION OF WASTE - ANALYSIS OF ELUATES - DETERMINATION OF PH, AS, BA, CD, CL[-], CO, CR, CR (6), CU, MO, NI, NO[2][-], PB, TOTAL S, SO[4][2-], V AND ZN
    NEN 7343 : 1995 LEACHING CHARACTERISTICS OF SOLID EARTHY AND STONY BUILDING AND WASTE MATERIALS - LEACHING TESTS - DETERMINATION OF THE LEACHING OF INORGANIC COMPONENTS FROM GRANULAR MATERIALS WITH THE COLUMN TEST
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