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DIN EN 13925-3:2005-07

Current

Current

The latest, up-to-date edition.

NON-DESTRUCTIVE TESTING - X RAY DIFFRACTION FROM POLYCRYSTALLINE AND AMORPHOUS MATERIALS - PART 3: INSTRUMENTS

Available format(s)

Hardcopy , PDF

Language(s)

English

Published date

01-01-2005

Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Description of equipment
   4.1 General
   4.2 X-ray sources
        4.2.1 General
        4.2.2 Conventional X-ray sources (sealed tubes
               and rotating anode sources)
        4.2.3 Synchrotron radiation sources
   4.3 Incident and diffracted X-ray beam optics
        4.3.1 General
        4.3.2 Monochromators
        4.3.3 Beam dimensions and geometry
   4.4 Detectors
        4.4.1 Types of detector
        4.4.2 Spatial resolution of detectors
        4.4.3 Energy resolution of detectors
   4.5 Goniometers
        4.5.1 General
        4.5.2 Specimen positioning
   4.6 Specimen stage
   4.7 Data collection system
5 Characterisation of equipment components
6 Equipment alignment and calibration
   6.1 General
   6.2 Alignment
   6.3 Calibration
7 Performance testing and monitoring
Annex A (informative) Relationship between the XRPD
        standards
Annex B (informative) Alignment of Bragg-Brentano
        diffractometers
Annex C (informative) Procedures for instrument performance
        characterisation
 C.1 General
 C.2 Position, intensity and breadth of a limited number
      of diffraction lines
 C.3 Angular Deviation Curve
 C.4 Line breadth
 C.5 Intensity diagrams
 C.6 Shape Analysis Curve
 C.7 Lattice parameters
 C.8 The use of the Fundamental Parameter Approach
 C.9 Whole pattern fitting
Annex D (informative) Sample report forms for characterisation
        of instruments
Bibliography

Defines the characteristics of instruments used for X-ray powder diffraction as a basis for their control and hence quality assurance of the measurements made by this technique.

DocumentType
Standard
Pages
42
PublisherName
German Institute for Standardisation (Deutsches Institut für Normung)
Status
Current

Standards Relationship
SN EN 13925-3 : 2005 Identical
BS EN 13925-3:2005 Identical
I.S. EN 13925-3:2005 Identical
UNE-EN 13925-3:2006 Identical
NF EN 13925-3 : 2005 Identical
NBN EN 13925-3 : 2005 Identical
EN 13925-3:2005 Identical
NEN EN 13925-3 : 2005 Identical
UNI EN 13925-3 : 2005 Identical
NS EN 13925-3 : 1ED 2005 Identical

ISO 5725-1:1994 Accuracy (trueness and precision) of measurement methods and results — Part 1: General principles and definitions
EN 13925-1:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous material - Part 1: General principles
EN 13925-2:2003 Non-destructive testing - X-ray diffraction from polycrystalline and amorphous materials - Part 2: Procedures

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