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ISO 15472:2010

Current

Current

The latest, up-to-date edition.

Surface chemical analysis X-ray photoelectron spectrometers Calibration of energy scales

Available format(s)

Hardcopy , PDF 1 User , PDF 3 Users , PDF 5 Users , PDF 9 Users

Language(s)

French, English

Published date

19-04-2010

ISO 15472:2010 specifies a method for calibrating the binding-energy scales of Xray photoelectron spectrometers, for general analytical purposes, using unmonochromated Al or Mg Xrays or monochromated Al Xrays. It is only applicable to instruments which incorporate an ion gun for sputter cleaning. It further specifies a method to establish a calibration schedule, to test for the binding-energy scale linearity at one intermediate energy, to confirm the uncertainty of the scale calibration at one low and one high binding-energy value, to correct for small drifts of that scale and to define the expanded uncertainty of the calibration of the binding-energy scale for a confidence level of 95 %. This uncertainty includes contributions for behaviours observed in interlaboratory studies but does not cover all of the defects that could occur. ISO 15472 is not applicable to instruments with binding-energy scale errors that are significantly non-linear with energy, to instruments operated in the constant retardation ratio mode at retardation ratios less than 10, to instruments with a spectrometer resolution worse than 1,5 eV, or to instruments requiring tolerance limits of 0,03 eV or less. It does not provide a full calibration check, which would confirm the energy measured at each addressable point on the energy scale and which would have to be performed in accordance with the manufacturer's recommended procedures.

DevelopmentNote
Supersedes ISO/DIS 15472. (04/2010)
DocumentType
Standard
Pages
30
PublisherName
International Organization for Standardization
Status
Current
Supersedes

Standards Relationship
NEN ISO 15472 : 2010 Identical
BS ISO 15472:2010 Identical
NF ISO 15472 : 2006 Identical

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ISO 19318:2004 Surface chemical analysis X-ray photoelectron spectroscopy Reporting of methods used for charge control and charge correction
BS ISO 19318:2004 Surface chemical analysis. X-ray photoelectron spectroscopy. Reporting of methods used for charge control and charge correction
ISO 20903:2011 Surface chemical analysis Auger electron spectroscopy and X-ray photoelectron spectroscopy Methods used to determine peak intensities and information required when reporting results
BS ISO 10810:2010 Surface chemical analysis. X-ray photoelectron spectroscopy. Guidelines for analysis
ISO 10810:2010 Surface chemical analysis X-ray photoelectron spectroscopy Guidelines for analysis
BS ISO 15470:2017 Surface chemical analysis. X-ray photoelectron spectroscopy. Description of selected instrumental performance parameters
ISO 13424:2013 Surface chemical analysis X-ray photoelectron spectroscopy Reporting of results of thin-film analysis
ASTM E 2735 : 2014 : REDLINE Standard Guide for Selection of Calibrations Needed for X-ray Photoelectron Spectroscopy (XPS) Experiments
10/30199175 DC : 0 BS ISO 16243 - SURFACE CHEMICAL ANALYSIS - RECORDING AND REPORTING DATA IN X-RAY PHOTOELECTRON SPECTROSCOPY (XPS)
BS ISO 13424:2013 Surface chemical analysis. X-ray photoelectron spectroscopy. Reporting of results of thin-film analysis
BS ISO 16243:2011 Surface chemical analysis. Recording and reporting data in X-ray photoelectron spectroscopy (XPS)
11/30230635 DC : 0 BS ISO 16129 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - PROCEDURES FOR ASSESSING THE DAY-TO-DAY PERFORMANCE OF AN X-RAY PHOTOELECTRON SPECTROMETER
BS ISO 24237:2005 Surface chemical analysis. X-ray photoelectron spectroscopy. Repeatability and constancy of intensity scale
ISO 16243:2011 Surface chemical analysis — Recording and reporting data in X-ray photoelectron spectroscopy (XPS)
PD ISO/TR 18196:2016 Nanotechnologies. Measurement technique matrix for the characterization of nano-objects
04/30109364 DC : DRAFT FEB 2004 ISO 24236 - SURFACE CHEMICAL ANALYSIS - AUGER ELECTRON SPECTROSCOPY - REPEATABILITY AND CONSTANCY OF INTENSITY SCALE
03/301547 DC : DRAFT JAN 2003 ISO 19318 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - REPORTING OF METHODS USED FOR CHARGE CONTROL AND CHARGE CORRECTION
04/30109361 DC : DRAFT FEB 2004 ISO 24237 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - REPEATABILITY AND CONSTANCY OF INTENSITY SCALE
18/30368969 DC : 0 BS ISO 16129 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - PROCEDURES FOR ASSESSING THE DAY-TO-DAY PERFORMANCE OF AN X-RAY PHOTOELECTRON SPECTROMETER
09/30191895 DC : 0 BS ISO 10810 - SURFACE CHEMICAL ANALYSIS - X-RAY PHOTOELECTRON SPECTROSCOPY - GUIDELINES FOR ANALYSIS
ASTM E 2108 : 2016 : REDLINE Standard Practice for Calibration of the Electron Binding-Energy Scale of an X-Ray Photoelectron Spectrometer
ISO/TR 18196:2016 Nanotechnologies — Measurement technique matrix for the characterization of nano-objects
ISO 15470:2017 Surface chemical analysis — X-ray photoelectron spectroscopy — Description of selected instrumental performance parameters
BS ISO 16129:2012 Surface chemical analysis. X-ray photoelectron spectroscopy. Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer
BS ISO 24236:2005 Surface chemical analysis. Auger electron spectroscopy. Repeatability and constancy of intensity scale
BS ISO 20903:2011 Surface chemical analysis. Auger electron spectroscopy and X-ray photoelectron spectroscopy. Methods used to determine peak intensities and information required when reporting results
ISO 16129:2012 Surface chemical analysis X-ray photoelectron spectroscopy Procedures for assessing the day-to-day performance of an X-ray photoelectron spectrometer
ISO 24237:2005 Surface chemical analysis — X-ray photoelectron spectroscopy — Repeatability and constancy of intensity scale

ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
ISO 7873:1993 Control charts for arithmetic average with warning limits
ISO 18115-1:2013 Surface chemical analysis — Vocabulary — Part 1: General terms and terms used in spectroscopy
ISO 7870-1:2014 Control charts Part 1: General guidelines

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