ASTM D 8274 : 2020 : REV A
Current
Current
The latest, up-to-date edition.
Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil by Portable Rapid Mid-Infrared Analyzer
Available format(s)
Hardcopy , PDF
Language(s)
English
Published date
01-10-2020
1.1This test method covers the determination of the content of biodiesel (fatty acid methyl esters (FAME)) in diesel fuel oils for volume fractions of 0.1 % to 31.0 % by mid-infrared analyzer with a resolution of 0.1 %.
Note 1:ASTM and ISO specification fuels falling within the scope of this test method include Specifications: D975 grades No. 1D and No. 2D, D7467, distillate grades of D396, MIL-DTL-16884, and distillate grades of marine fuel specification ISO 8217.
1.2The accuracy of this test method is based on the molecular weight of C16 and C18 FAME species.
1.2.1Discussion—Biodiesel contains a variety of species with different molecular weights. Typical market FAMEs from North America and Europe, which are predominantly soy, rapeseed, and used cooking oil derived FAME were included in the pilot study. FAME derived from coconut, which predominantly contains C12, will over-read by approximately 30 %.
1.3This method cannot distinguish between vegetable oils, animal fats, FAEE, compounds containing carbonyl groups, and FAME. For more information, see Section 6.
1.4This test method has interim repeatability precision only, see Section 14 for more information.
1.5The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.7This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
| Committee |
D 02
|
| DocumentType |
Test Method
|
| Pages |
6
|
| PublisherName |
American Society for Testing and Materials
|
| Status |
Current
|
| Supersedes |
| ASTM D 4057 : 2019 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 7467 : 2023 | Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20) |
| ASTM D 7797 : 2023 | Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 4175 : 2020 : REV B | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 396 : 2020 | Standard Specification for Fuel Oils |
| ASTM D 86 : 2023 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 7467 : 2009 | Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20) |
| ASTM D 7371 : 2014 | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method) |
| ASTM D 7371 : 2014 : R2022 | Standard Test Method for Determination of Biodiesel (Fatty Acid Methyl Esters) Content in Diesel Fuel Oil Using Mid Infrared Spectroscopy (FTIR-ATR-PLS Method) |
| ASTM D 975 : 2022 | Standard Specification for Diesel Fuel |
| ASTM D 86 : 2023 : REV A : EDT 1 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 86 : 2020 : REV A | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 7963 : 2022 | Standard Test Method for Determination of Contamination Level of Fatty Acid Methyl Esters in Middle Distillate and Residual Fuels Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 4052 : 2018 : REV A | Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter |
| ASTM D 1298 : 2012 : REV B : R2017 : EDT 1 | Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method |
| ASTM D 396 : 1998 | Standard Specification for Fuel Oils |
| ASTM D 6299 : 2021 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 975 : 2019 : REV B | Standard Specification for Diesel Fuel |
| ASTM D 86 : 2018 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 4175 : 2022 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6299 : 2022 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 1298 : 2012 : REV B : R2017 | Standard Test Method for Density, Relative Density, or API Gravity of Crude Petroleum and Liquid Petroleum Products by Hydrometer Method |
| ASTM D 445 : 2021 : EDT 2 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 975 : 2021 | Standard Specification for Diesel Fuel |
| ASTM D 975 : 2023 : REV A | Standard Specification for Diesel Fuel |
| ASTM D 445 : 2017 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 6299 : 2023 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4175 : 2001 : EDT 1 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 4175 : 2020 : REV B : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 86 : 2019 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 4175 : 2022 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6300 : 2021 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4175 : 2002 | Standard Terminology Relating to Petroleum, Petroleum Products, and Lubricants |
| ASTM D 86 : 2012 | Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure |
| ASTM D 6300 : 2023 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 445 : 1988 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and the Calculation of Dynamic Viscosity) |
| ASTM D 975 : 2020 : REV C | Standard Specification for Diesel Fuel |
| ASTM D 4175 : 2023 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 7963 : 2021 | Standard Test Method for Determination of Contamination Level of Fatty Acid Methyl Esters in Middle Distillate and Residual Fuels Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 6300 : 2023 : REV A | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6300 : 2020 : REV B | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 6299 : 2023 : EDT 1 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 7963 : 2019 : EDT 1 | Standard Test Method for Determination of Contamination Level of Fatty Acid Methyl Esters in Middle Distillate and Residual Fuels Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 4175 : 2022 : REV A : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 86 : 2020 : REV B | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 86 : 2016 : REV A | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 6300 : 1999 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products and Lubricants |
| ASTM D 445 : 2019 : REV A | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 4177 : 2022 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 6751 : 2023 : REV A | Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels |
| ASTM D 6299 : 2023 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 6751 : 2020 : REV A | Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels |
| ASTM D 4307 : 2017 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 445 : 2019 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 4175 : 2023 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4052 : 1996 | Standard Test Method for Density and Relative Density of Liquids by Digital Density Meter |
| ASTM D 4175 : 2023 : REV A | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 4307 : 2017 : R2021 | Standard Practice for Preparation of Liquid Blends for Use as Analytical Standards |
| ASTM D 4175 : 2022 : EDT 1 | Standard Terminology Relating to Petroleum Products, Liquid Fuels, and Lubricants |
| ASTM D 86 : 2023 : REV A | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 975 : 2022 : REV A | Standard Specification for Diesel Fuel |
| ASTM D 396 : 2021 | Standard Specification for Fuel Oils |
| ASTM D 445 : 2001 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (the Calculation of Dynamic Viscosity) |
| ASTM D 6751 : 2023 | Standard Specification for Biodiesel Fuel Blend Stock (B100) for Middle Distillate Fuels |
| ASTM D 6299 : 2022 | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 396 : 2009 | Standard Specification for Fuel Oils |
| ASTM D 445 : 2024 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 445 : 2021 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 86 : 2020 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 4057 : 2022 | Standard Practice for Manual Sampling of Petroleum and Petroleum Products |
| ASTM D 975 : 2023 | Standard Specification for Diesel Fuel |
| ASTM D 4052 : 2022 | Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter |
| ASTM D 4177 : 2020 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 445 : 2018 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 86 : 2015 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 445 : 2021 : EDT 1 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 6299 : 2020 : REV A | Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance |
| ASTM D 4177 : 2022 : EDT 1 | Standard Practice for Automatic Sampling of Petroleum and Petroleum Products |
| ASTM D 7467 : 2020 : REV A | Standard Specification for Diesel Fuel Oil, Biodiesel Blend (B6 to B20) |
| ASTM D 86 : 2017 | Standard Test Method for Distillation of Petroleum Products and Liquid Fuels at Atmospheric Pressure |
| ASTM D 7797 : 2018 | Standard Test Method for Determination of the Fatty Acid Methyl Esters Content of Aviation Turbine Fuel Using Flow Analysis by Fourier Transform Infrared Spectroscopy—Rapid Screening Method |
| ASTM D 445 : 2023 | Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) |
| ASTM D 6300 : 2024 | Standard Practice for Determination of Precision and Bias Data for Use in Test Methods for Petroleum Products, Liquid Fuels, and Lubricants |
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